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COLUMBIA ANALY'T'ICAL SERVICES,INC <br /> QA/QC Report <br /> Client @qurva Services Service Request 59901977 <br /> Protect SAP 121258/Incident 88870583 Date Collected 6/29/99 <br /> Sample Matrix Soil Date Received 6/30/99 <br /> Date Extracted 6/30/99 <br /> Date Analyzed 7/5/99 <br /> Matrix Spike/Duplicate Matnx Spike Summary <br /> TPH as Gasoline <br /> Sample Name SP-1A Units mg/Kg(ppm) <br /> Lab Code 59901977-001MS, 59901977-OOIDMS Basis Wet <br /> Test Notes <br /> Percent Recovery <br /> CAS Relative <br /> Prep Analysis Spike Level Sample Spike Result Acceptance Percent Result <br /> Analyte Method Method MRL MS DMS Result MS DMS MS DMS Limits Difference Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 1 10 10 ND 10 11 I00 110 67-121 10 <br /> 0 <br /> Approved By Dater / <br /> DMSM20597p • <br />