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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client Equiva Smirl es Service Request: K9904880 <br /> Protect Incident# 88870583/SAP#121258 Date Collected: 6/29/99 <br /> Sample Matrix Soil Date Received: 6/30/99 <br /> Date TCLP Performed: 7/27/99 <br /> Date Extracted: 7/28/99 <br /> Date Analyzed: 812/99 <br /> Toxicity Charac.teristw Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Metals <br /> Sample Name SP-16AB COMP Units mg/L(ppm) <br /> Lab Code K9904880-052 Basis NA <br /> Test Notes <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Lead EPA 3010 6010B 005 1 5 ND <br /> i <br /> * From 40 CFR Part 261,et al,and Federal Register,March 29, 1990 and June 29,1990 <br /> Approved By Date <br /> 1S44l052595 <br /> Page 9 <br />