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COLUMBIA ANALYTICAL SERVICES,INC <br /> Analytical Report <br /> Client. Equiva Services Service Request K9904880 <br /> Protect Incident# 88870583/SAP4121258 Date Co11eLted 6129/99 <br /> Sample Matrix Sol] Date Received 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed 812/99 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Metals <br /> Sample Name SPA 7AB COMP Units mg/1-(ppm) <br /> Lab Code K9904880-053 Basis NA <br /> Test Notes <br /> Prep Analvsis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Lead EPA 3010 6010E 005 1 5 ND <br /> I <br /> * From 40 CFR Part 261,et al,and Federal Register,March 29 1990 and June 29, 1990 <br /> Approved By Date <br /> 1544/652595 <br /> Page 10 <br />