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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: Equiva Strvices Service Request K9904880 <br /> • Project: Incident# 88870583/SAP#121258 Date Collected NA <br /> Sample Matrix Soil Date Received. NA <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted 7/28/99 <br /> Date Analyzed 812199 <br /> Toxicity CharaLteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Metals <br /> Sample Name Method Blank Units mg/L(ppm) <br /> Lab Code K9904890-MB Basis NA <br /> Test Notes <br /> Prep Analysts Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Lead EPA 3010 6010E 005 1 5 ND <br /> From 40 CFR Part 261,et al and Federal Reg7ster,March 29, 1990 and June 29 1990 <br /> Approved By Date 1w- <br /> IS441052595 <br /> Page 12 <br />