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COLUMBIA ANALYTICAL SERVICES,INC. <br /> QA/QC Report <br /> Client: Equiva Services Service Request K990488o . <br /> Project* Incident# 88870583/SAPlt121258 Date Collected 6/29/99 <br /> Sample Matrix Soil Date Received: 6/30/99 <br /> Date TCLP Performed 7/27/99 <br /> Date Extracted. 7128199 <br /> Date Analyzed 8/2/99 <br /> Matrix Spike Summary <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Metals <br /> Sample Name SP-IAB COMP Units mg/L(ppm) <br /> Lab Code K9904880-037MS Basis NA <br /> Test Notes <br /> Spiked <br /> Peep Analytiis Spike Sample Sample Percent Result <br /> Analyte Method Method MRL Level Result Result Recovery* Notes <br /> Lead EPA 3010 6010A 005 5 0 ND 436 87 <br /> * Percent recovery intormation is provided in order to asses~the performance of the method on this matna <br /> LApproved By Date <br /> MS/031695 <br /> Page 13 <br />