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I 10 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 http/twwwmecampbellcom E-mail mam@mccampbell cam ' Advanced GeoEnvironmental Client Project ID K &S Gas&Grocery Date Sampled 11/02/01 837 Shaw Road Date Received 11/06/01 ' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11113-11/14/01 Client P O Date Analyzed 11/13-11/14101 Volatile Organics By GUMS — EPA method 5260 — Lab ID 52829 ' Client ID 1 CPT-4-54 Matrix Repomng Limit kepo nng Limit ' Compound Concentration* W Compound– � Concentration*-- — - - S 1 S Acetone @' ND<500 50 25 trans-1 3-Dichlaropropene I N )<100 1 0 5 0 Benzene 1 3500 10 5 0 Ethylene dibromideND<100 1 0 50 Bromobenzene ND<100 10 50 1 Ethylberizene 640 1 0 50 ' Bromochloromethane ND<l 00 _10 50 I-lexachlorobutadtene ND<500 50 25 Bromodichloromethane i ND<100 1 0 50 Iodomethane ND<100 10 50 Bromoform ND<100 1 0 50 Isopropylbenzene N13<100 1 0 50 Bromomethane ND<100 1 0 50 p-lsopropyl toluene ND<l 00 1 U 50 ' n-Butyl benzene ND<100 1 0 50 Methy butyl ketone ND<100 1 0 5 0 sec-Butyl benzene ND<100 L 10 50 Methylene Chionde` ND<100 �, 0 5 0 tert-Butyl benzene ND<100 10 50 Methyl ethyl ketone ND<200 20 10 Carbon Disulfide ND<100 10 50 Methyl isobutyl ketones ND<l 00 16 50 Carbon Tetrachiorrdc NF)--100 10 50 Methyl tert-Butyl Ether(MTBE) -- 1 0 1, 50 Chlorobenzene ND<100 10 50 Naphthaiene ND<100 50 '7 0 Chloroethane ND<100 i 1 0 i 50 n-Propyl benzene ND<100 1 0 U 2-Chloroethyl Vinyl lather` ND<100 1 0 j 50 Styrene I ND<100 1 0 5 0 1 Chloroform ND<100 1 0 i 50 1 1,1,2-Tetrachloroethane ND<100 1 0 50 Chiorumethane ND<]00 l Q so 1,1,2,2-Tetrachloroethane ND<]00 1 0 50 2-Chlorotoluene ND<100 1 0 50 Tetrachloroethene ND<100 10 50 4-Chlorotoluene ND<100 10 50 Toluene ND<]00 1 0 50 Dibromochloromethatte ND<100 1 0 50 12,3-Tnchlorobenzene ND<500 50 25 1 2-Dibromo-3-chloroproparte ND<200 20 10 1,2 4-1 nchlorobenzene ND<500 50 25 Dibromomethane ND<100 10 50 1,1,1-Tnchloroethane ND<100 10 150 1,2-Dichlorobenzene ND<100 1 0 50 1,1,2-Tnchloroethane ND<100 10 1 1,3-Dichlorobenzene NIK100 10 5 0 Trichloroethene ND<100 ] 0 1 4-Dichlorobenzene ND<100 10 50 Tnehlorofluoromethane ND<l 00 1 0 Dichlorodifluoromethane ND<100 to 50 1,2,3-Tnchloropropane ND<100 10 50 1,1-Dichloroetl ND<100 10 50 1,2,4-Trimethylbenzene ND<100 1 0 50 ' 1 2-Dichloroethane ND<100 10 50 1 3,5-Tnmethylbenzene ND<100 1 0 50 1,1-Dichloroethene ND<100 1 0 50 Vinyl Acetate ND<100 50 25 cis-1,2-Dichloroethene ND<100 10 50 Vinyl Chloride ND<100 1 0 50 trans-l,2-Dtchloroethene ND<100 10 50 Xyienes,total 660 1 0 50 ' 1 2-Dichloropropane ND<100 10 50 Comments 1,3-Dichloropropane ND<100 1 0 50 Surragate Recoveries(%) 2,2-Dichioropropane ND<100 1 0 50 Dibromofluoromethane 116 1,1-Dichioropropene ND<100 10 50 Toiuene-d8 100 cis-1 3-Dichloropropene ND<100 1 0 50 4-13romofiuorobenzene 101 water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ' ND means not detected above the reporting limit N/A means analyte not applicable to this analysis (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanotie, (e) dichloromethane, (f) 2-butanone (g) 4-methyl-2- pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than –5 vol 0/0 seotment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) chloroethene,(o)dimethylbenzenes DHS Certification No 1644 Edward Hamilton,Lab Director