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' 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 http//www mccampbell com E-mail main@mccampbell com ' Advanced GeoEnvironmental Client Project ID K & S Gas&-Grocery Date Sampled 11/02/0I 837 Shaw Road Date Received 11/06/01 ' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11113-11/14/01 Client P O Date Analyzed 11113-11/14101 Volatile Organics By GC/MS EPA method 8260 _ _ Lab ID 82830 ' Client ID CPT-4-81 — Matrix � W_ _ Reporting lama � Report:ng Limit Compound Concentration* W S Compound Concentrations W �5 ' Acetone roi ND<25 5 0 25 trans-l,3-Dichloropropene ND<5 0 I Q �5 0 Benzene 200 1 0 50 Ethylene dibromide ND<5 0 10 1 50 Bromobenzene ND<5 0 10 50 Ethylbenzene ZND<5 10 50 ' Bromochloromethane ND<5 0 10 50 Hexachlorobutadiene 50 25 Bromadichlorometnane ND<5 0 1 0 5 0 Iodometbane 1 0 5 0 Bromoform ND<S 0 1 0 5 0 lsopmpylbenzene 1 6 56 Bromomethane ND<5 0 1 0 5 0 p-Isopropyl toluene 0 5 0 ' n-Butyl benzene ND<5 0 1 0 5o Methyl butyl ketone ND<5 0 1 0 50 sec-Butyl benzene ND<5 0 1 0 50 1 Methylene Chloride" i ND<5 0 1 0 5 0 tent-Butyl benzene ND<5 0 1 0 50 Methyl ethyl ketone ND<10 2 0 10 Carbon Disulfide ND<5 0 1 0 50 Methyl isobutyl ketone ` ND<5 0 1 0 5c ' I Carnor Tetrachloride ND<5 0 1 0 50 Methyl tori-Butyl Fther(MTRF) -- 1 0 5 0 Chlorobenzene ND<5 0 1 0 5 0 'Naphthaieni. ND<5 0 5 0 5 0 Chloroethane ND<5 0 I Q 50 J n-Propyl benzene ND<5 0 1 0 i f 2 Chiomethyl Vmy Ether"' N5<5 6 1 0 50 Styrene ND<5 0 1 0 so ' Chloroform ND<5 0 0 50 1,1 ,2-Tetrachloroethane ND<5 0 1 0 1 5( Chloromethane ND<5 0 1 0 50 1 1,2,2-Tetrachioroethanc ND<5 0 1 0 5(, 2-Chiorotoluene ND<5 0 1 0 50 Tetraahiciroethene ND<5 0 1 0 5 0 4-Chiorotoluene ND<5 0 1 0 5 0 Toluene ' ND<5 0 1 0 50 Dibromochloromethane ND<5 0 1 0 5 0 1 1,2,3-Tnchlorobenzene ND<25 5 0 25 1.2-Dibromo-3-chloropropane ND<10 2 0 10 1 1 2,4-Trichlorobenzene ND<25 50 25 Dibrornomethane ND<5 0 1 0 50 1,1,1-Trichloroethane ND<5 0 1 0 5 0 1,2-Dichlorobenzene ND<5 0 1 Q 5 0 1,42-Tnchloroethane ND<5 0 1 0 5 Q ' 1 3-Dichiorobenzene ND<5 0 10 5 Q 1 Tnchloroethene ND<5 0 1 0 50 1,4-Dichlorobenzene ND<5 0 1 0 so Tnchlorofluoromethane ND<5 0 1 0 5 0 Dichlorodifluoromethane ND<5 0 10 50 1 2,3-Tnchloropropane ND<5 0 1 0 5( ' 1,1-Dichloroethane ND<5 0 10 50 1 2,4-Tnmethylbenzene ND<S 0 1 0 50 1 2-Dichloroethane ND<5 0 1 0 50 1,3 5-Trimethylbenzene ND<5 0 1 0 50 1,1-Dichloroethene ND<5 0 1 0 5 0 Vinyl Acetate m ND<25 50 25 cis-1,2-Dichloroethene ND<5 0 1 0 50 Vinyl Chionde " ND<5 0 1 0 5 0 ' trans-l,2-Dicbloroethene ND<5 0 1 0 5 0 Xyienes,total ND<5 0 10 5 0 1,2-Dichloropropane ND<5 0 1 0 5 0 Comments i,3-Dichloropropane ND<5 0 1 0 50 Surrogate Recoveries(%) 2,2-Dichloropropane ND<5 0 1 0 1 50 Dibmmofluoromethane 116 ' 1,1-Dichloropropene ND<5 0 10 1 5 0 Toluene-d8 – 99 cis-1,3-DichloropropeneND<5 0 1 0 5 0 4-Sromofluorobenzene 101 water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ' ND means not detected above the reporting]trent NIA means analyte not applicable to this analysts (b) 2-propanone or dimethyl ketone, (c) (2-chloroetboxy) ethene (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- pentanone or isopropylacetone, (b)lighter than water immiscible sheen is present, (t) liquid sample that contains greater than --5 vol % sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, 0) methylbenzene (m) acetic acid ethenyl ester, (n) ' chloroethene,(o)dimethylbenzenes DHS Certification No 1644 Edward Hamilton, Lab Director