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' 110 2nd Avenuc South t#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 h //www mccam bell com E-mail main@ necampbell eom Advanced GeoEnvironmental Client Project ID K&S Gas &Grocery Date Sampled 11/07/01 837 Shaw Road Date Received 11/09/01 ' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11114-11116101 Client P O Date Analyzed 11/14-11/16/01 ' V Volatile Organics By GC/MS EPA method 8260 --— -- Lab ID 83352 ' Client ID CPT-5-1 11 — Matrix W Rcpom g Limit * Reporting Limit Concentration* W S Compound Concentration W S - ' Acetone'bj ND<505 0 25 trans-1 3-Dichloropropene ND<5 0 1 0 50 Benzene 120 1 0 5 0 Ethylene dibromide ND<5 0 1 0 50 Broinobenzene ND<5 0 1 0 5 0 Ethylbenzene 99 to 1 50 Bromochloromethane ND<5 Q ] 0 5 0 Hexachlorobutadiene ND<25 50 25 Bromodichloromcthane ND<5 0 1 0 5 0 Iodomethane �i ND<5 0 l 0 50 Bromoform ND<5 0 10 5 0 lsopropylbenzene ND<5 0 1 0 50 Bromomethane ND<5 0 10 5 0 p-Isopropyl toluene ND<5 0 10 1 5 0 ' n-Butyl benzene ND<5 0 1 01 5o Methyl butyl ketone ND<5 0 1 0 1 5 0 sec-Butyl benzene ----RD—<50 10 1 5 0 Methylene Chloride" ND<10 1 0 5 0 ter, Butyl benzene ND<5 0 1 0 5 0 i Methyl ethyl ketone` ND<10 2 0 10 Carbon Disulfide ND<5 0 1 0 5 0 Methyl isobutyl ketones ND<5 0 0 50 Carbon Tetrachloride ND<5 0 1, 10 50 Methyl tert-Butyl Ether(MTBE) -- 1 0 50 i Chlorobenzene NIKS 0 10 5 0 'naphthalene ND<25 50 2s Chloroethane ND<5 0 1 0 5 0 n-Propyl benzene ND<5 0 l 0 5 0 2-Chloroethyi Vinyl Ethe ---VD—<50 10 5 0 Styrene ND<5 0 0 56 Chloroform ND<5 0 10 50 1,1 1,2-Tetrachloroethane ND<5 0 ~ , 0 5 C Chloromethane ND<5 0 1 0 50 1,1,2 2-Tetrachloroethane ND<5 0 10 50 2-Chlorotoluene ND<5 U 1 1 0 5 0 Tetrachloroethene ND<5 0 1 0 5 0 4-Chlorotoluene ND<5 0 1 0 5 0 Toluene ' ND<5 0 1 0 5 0 Dibromochloromethane ND<5 0 1 0 5 0 1 2 3-1 nchlorobenzene ND<25 5 0 20 1,2-Dibiamo-3-chloropropane ND<10 2 0 10 1,2,4-Tnchlorobenzene ND<25 50 25 Dibromomethane NIK5 0 —T-6 . 5 0 1,1,1-Inchloroethane ND<5 0 1 0 50 1,2-Dichlorobenzene ND<5 0 10 5 0 1 1,2-Tnchloroethane ND<5 0 1 0 50 ' [11-Dichlorobenzene ND<5 0 1 0 5 0 Trichloroethene ND<5 0 16- 50 1 4-Dichlorobenzene ND<5 0 1 0 50 Tnehlorofluoromethane ND<5 0 1 0 5 0 Dichlorodifluoromethane ND<5 0 10 5 0 1,2,3-Tnchloropropane ND<5 0 1 0 5 0 1 1-Dichloroethane ND<5 0 10 5 0 1,2,4-Tnmethylbenzene ND<5 0 1 0 50 1,2-D3chloroethane ND<5 0 1 0 5 0 1,3 5-Tnmethylbenzene ND<5 0 1 0 5 0 1,1-Dichloroethene ND<5 0 1 0 50 Vinyl Acetate`� ND<25 5 0 25 cis-1,2-Dichloroethene ND<5❑ 1 0 5 0 Vinyl Chloride ") ND<5 0 1 0 5 0 trans-1 2-Dichloroethene ND<5 0 1 0 5 0 Xylenes,total ° NIKS 0 1 0 5 4 1,2-Dichloropropane ND<5 0 1 0 5 0 Comments 1,3-Dichloropropane ND<5 0 1 0 5 0 Surrogate Recoveries(%) 2,2-Dichloropmpane ND<5 0 10 5 0 Dibromofluoromethane 123 1 1-Dichloropnopene ND<5 0 1 0 5 0 Toluene-d8 101 ' cis-1,3-Dichloropropene ND<5 0 10 5 0 4-Bromofluoronenzme 98 water and vapor samples are reported in ug(L,soil and sludge samples in ug/kg wipes in ug/wipe and al,TCLP/SPLP extracts in ug/L ' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (t) 2-butanone, (g) 4-methyl-2- pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i) liquid saruple that contains greater than —5 vol % sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) ' chloroethenc,(o)dimethylbenzenes DHS Certification No 1644 Edward Hamilton,Lab Director