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116 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@rnccampbell corn <br /> Advanced GeoEnvtronmental Client Proj ect ID K&S Gas&Grocery Date Sampled 11/07/01 <br /> 837 Shams Road <br /> Date Received 11/09/0I <br />' Stockton, CA 95215 Client Contact Calvin Lee � Date Extracted 11114-11/16/01 <br /> Client P O Date Analyzed 11/14-11/16/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID s 83353 <br /> JClient ID -- CPT-5-128 — <br /> _Matrix 1' _ <br /> �� T� Rcpomng 4�mst I � I K Rspmmng Limn <br /> Compound Concentration* Compound II Concentration <br /> Acetone WX10 5 D 25 trans-1 3-Dichloropropene ND <br />' Benzene 9 8 1 0 50 Ethylene dibromidi I ND 1 0 5 0 <br /> Bromobenzene ND 1 0 50 &thvlbenzene 43 1 0 5 0 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 5 0 25 <br /> 1 Bromodichloromethane ND 1 0 50 lodomethane ND 1 0 50 <br /> Bromoform ND 1 0 5 0 lsopropylbenzene 4 0 1 0 5 6 <br /> B�romomeI�hane ND ] 0 7 50 p-lsopropyl toluene ND 1 0 1 4 C <br /> n-Butyl I benzene 3 3 1 0 5 0 Methyl butyl ketene 1d ND �1�0__,1 5 0 <br /> t SLc-Butyl benzene N— - 1 l 1 0 5 0 Methvlene Chloride" ND 1 0 <br /> tert-Butyl benzene ND 10 1 5 0 Methvl ethyl ketone" ND 2( 10 <br /> IleCarbon Disulfide ND 1 0 5 0 Methv isobutyl ketone i ND 1 0 7 5 0 <br /> Carbon Tctrachlonde ND 10 50 Methyl tent-Butyl Ether(MTBE) — lo 50 <br /> Chlorobenzene ND 1 0 5 0 Naphthalene 12 50 25 <br /> Chloroethane ND 10 5 0 —n-Propyl benzene 12 10 5 0 <br /> 2-Chloroethyl Vinyl Ether"' ND 1 0 0 Styrene tk ND 1 10 5 0 <br /> Chloroform ND 1 0 5 0 1,1 12-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND ] 0 5 0 1,1 2,2-Tetrachloroethane ND 1 0 5 0 <br /> 1 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene t'} 1 0 3 5 0 <br />' Dibromochloromethane ND 10 50 1 2,3-Tnchlorobenzene ND 5 0 25 <br /> 1.2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 2' <br /> Dibromomethane ND 10 5 0 1 ),1-Trichloroethane ND 10 5 0 <br /> i 2-Dichloroben4ene ND ] 0 50 1,1 2-Trichloroethane ND 1 0 5 0 <br /> 1,3-Dichlorobenzene ND 10 50 Tnchloroethene ND 1 0 50 <br /> ' 4-DichlorobenzeneND 1 0 5 0 Tnehlorofluoromethane ND 1 0 50 <br /> Dichlorodifluoromethane ND 10 50 1 2 3-Tnchloropropane ND 10 5 0 <br /> 1 1-Dichloroethane ND 1 0 5 0 1,2,4-Trimethylbenzene 55 10 50 <br /> 1 2-Dichloroethane ND 1 0 50 1 3 5-Tnmethylbenzene ND 10 5 0 <br /> 1 1-Dichloroethene ND 1 0 5 0 Vinyl Acetate t" ND 50 25 <br /> cis-1 2-Dichloroethene ND 10 5 0 Vinyl Chloride"' ND 1 0 5 0 <br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total 190 1 0 5 0 <br />' 1 2-Dichloropmpane ND 1 0 5 0 Comments <br /> 1,3-Dichlaro ro ane ND 1 0 I 5 0 Surro ate Recoveries <br /> 2 2-Dichloropropane ND J 10 5 0 Dibromofluoromethane 126 <br /> 1,1-Dichloropmpene ND 1 0 5 0 Toluene-d8 99 <br /> cis-1,3-DichloropLoyene. ND 1 0 5 0 4-Bromottuorobenzene 96 <br /> water and vapor samples are reported in ug/L. soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting hunt,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (r) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> ' chloroethene o dimethylbenzenes <br /> DHS Certification No 1644 Edward Harnilton,Lab Director <br />