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i <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbcll com E-mail main r�1i mccampbell com <br />' I <br /> Advanced Geo)wnvironmenta] Client Project ID K&, S Gas &Grocery Date Sampled 11/07/01 <br /> 837 Shaw Road ! Date Received 11/09/01 <br /> t1I Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 11/14-11/16/01 <br /> I <br /> Client P O Date Analyzed 11/14-11/16/01 <br /> Volatile Organics By GUMS <br /> EPA method 8260 _ <br /> Lab ID--T83354 <br /> Client 1D — CPT-5-143 <br /> Matrix W <br /> * Reporting Limit Rcponmg Limn <br /> Compound Concentration w S Compound I Concentration 5 <br /> Acetone t" ND<10 5 0 25 trans-l,3-Dichloropropene 3nrD 10 "0 <br /> Benzene 4 9 10 5 0 Ethylene dibromide ND to so <br /> Bromobenzene ND 10 50 Ethvlbenzene 1 9 . 1 0 50 <br />' Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> BrOmOdichloromethane ND 1 0 l 50 lodomethane ND 1 0 50 <br /> Sromafarm ND to 50 lsonropylbenzene ND 1 0 50 <br /> Bromomethane ND 10 1 50 p-isopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND l 0 50 Methvl butvl ketone{d' ND 1 0 50 <br /> sec-Butyl benzene ND 1 C 5 0 Methylene Chloride" ND t 0 50 <br /> ten-Butyl benzene ND l SO i N ethy ethyl ketone `' ND 20 '0 <br /> Carbon Disulfide ND 0 50 Methyl isobutyl ketone es ND 1 0 50 <br /> Carbon Tetrachloride ND 0 5 0 ~tthyl ten-Butvl Ethcr(MTBE) l 0 =5( <br /> Chiorobenzene ND 10 50 ]naphthalene ND 5 0 2� <br /> I Chloroethane ND l 0 50 n-Propyl benzene ND 1 0 50 <br /> 2-Chloroethyl Vinyl Ether(` ND 1 G 50 Styrene ND ' 0 50 <br />' Chloroform ND l 0 50 i 1,1 1 2-Tetrachloroethane ND 1 0 50 <br /> Chloromethane ND —to 5 0 1,1,-- 2-Tetrachloroethane i ND 10 50 <br /> 2-Chlorotoiuene ND 10 50 Tetrachioroethene ND 1 0 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene 12 10 50 <br />' 1 Dibromochloromethane ND 10 50 1 2,3-Tnehiorobenzene ND 50 25 <br /> 2-Dibromo-3�hloropropane ND 20 10 1 2 4-rnchlorobenzene ND 50 25 <br /> Dibromomethane ND i 10 50 1,' l-Trichloroethane ND 1 0 50 <br />' 1 2-Dichlorobenzene ND 1 0 50 1,1 2-Tnchioroethane ND 1 0 5 0 <br /> 1 3-Dichlorobenzene ND 1 0 5 0 3nchloroethene ND 1 0 50 <br /> 4-Dichlorobenzene ND 10 50 Tri ehlOroflnOTOmethane ND 1 0 1 50 <br /> Dichlorodifluoromethane ND 10 50 1,2 3-Tnchloropropane ND 10 5 0 <br /> I i-Dichloroethane ND 10 5o 2 4-Tnmethylbenzene ND 1 0 50 <br /> 1 2 Dichloroethanc ND 10 50 3 5-7nmethyibenzene ND 1 0 50 <br /> I l-Dichloroethene ND 10 so Vinyl Acetate 1m° ND 50 1 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride"' ND 1 0 50 <br />' trans-l,2-Dichiomethene ND 10 50 Xylenes total 70 1 0 50 <br /> 1 2-Dichloroprapane ND 1 0 5 0 Comments <br /> 1 3-Diehl aro ro ane ND 1 0 50 Surrogate Recoveries <br /> 2 2-Dichloropropane ND 1 0 50 Dibromofluoromethanc 120 <br />' <br /> IJ-Dichloropropene ND 1 0 5 0 Toluene-d8 102 <br /> cis-1,3-Dichloro rapene ND 1 0 5 0 4-Bromofluorobenzene 104 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanorie or isopropylacetone (h) lighter than water immiscible sheen is present, ()) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene, o dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />