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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccatn bell corn E-mail mam@mccampbell corn <br />' <br /> Date Sampled 02/l4/O1 <br /> Advanced GeoEnvironmental Client Project ID K& S Gas& Grocery <br /> Date Received 02/20/01 <br /> 837 Shaw Road <br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/20-02/22101 <br /> Client P O Date Analyzed 02120-02/22/01 <br />' Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br /> Lab 1D Client 1D Matrix TPH(g)* MTBE Benzene Toluene Ethyl Xylenes %Recovery <br /> benzene Surrogate <br /> 60453 P-1/65 W 4000,a ND<20 630 170 64 370 104 <br /> 60454 P-1/82 W 1400,a ND 320 26 50 51 108 <br /> I <br /> 60455 P-1195 W 120,a ND 20 78 31 14 100 <br /> I60456 P-1/73-74 S ND ND ND ND ND ND 102 <br /> 60457 P-2/65' W 190,a ND 21 11 ND 17 104 <br />' 60458 P-2/81' W 110,c ND 86 I 1 ND ND 108 <br /> 60459 P-2/93' W ND ND 37 ND ND ND 96 <br /> 60460 P-2/71-72' S ND ND ND ND ND ND 107 <br /> 60461 P-3/3040' W I 10,c ND 21 3 8 ND 053 102 <br /> 60462 P-3155-60' W 4900,a ND<I0 710 28 82 44 113 <br />' 60463 P-3/77-81' W ND ND ND ND ND ND 98 <br /> 60464 P-3/95-97' W ND ND ND ND ND ND 92 <br /> I 60465 P-3/117 W 1100,a ND 280 11 34 11 lit <br /> 121' <br />' Reporting Limit unless W 50 ug/L 50 05 0 5 05 05 <br /> otherunse stated,ND <br /> means not detected above <br /> the reporting limitS 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br /> I *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> "cluttered chromatogram,sample peak coelutes with surrogate peak <br /> 'Thc following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br /> gasohne?) c) lighter gasoline range compounds (the most mobile fracimn) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant,biologically altered gasoline),e)TPH pattern that does not appear to be derived from gasoline (?) f) <br /> one to a few isolated peaks present,g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible <br /> she is present,i)liquid sample that contains greater than--5 vol %sediment,3)no recognizable pattern <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />