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1102nd Avenue South,#137,Pacheco,CA 94553-5560
<br /> McCAMPRELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//wwwmgqMpbe1lconi E-mail main@mccampbell com
<br /> NAdvanced GeoEnvironmental Client Project ID K&S Gas& Grocery Date Sampled 02/14/01
<br /> 837 Shaw Road Date Received 02/20/01
<br />' Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02121-02/28101
<br /> Client P Q Date Analyzed 02/21-02/28/01
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> I Lab ID 60453
<br /> Client ID P-1/65
<br /> Matrix W
<br /> Compound Concentration* Rung Lei Compound Concentration* xeporong Limn
<br />' W S W S
<br /> Acetone ro ND<20 50 25 trans-1,3-Dichlompropene ND<10 10 50
<br /> Benzene 710 10 5 0 Ethylene dibromide ND<10 1 0 50
<br /> Bromobenzene ND<10 10 5 0 Ethylbenzene 47 1 0 5 0
<br /> Bromochloromethane ND<lO 10 5 0 Hexachlorobutadiene ND<10 5 0 25
<br /> Bromodichloromethane ND<l 0 10 50 Iodomethane ND<10 1 0 1 5 0
<br /> Bromaform ND<10 1 0 5 0 Isopropylbenzene 21 1 0 5 0
<br /> Bromomethane ND<10 10 50 p-Isopropyl toluene ND<10 1 0 5 0
<br /> n-Butyl benzene ND<10 10 5 0 Methyl butyl ketone N13<10 1 0 5 0
<br /> sec-Butyl benzene ND<10 10 5 0 Methylene Chloride"' ND<I O 1 0 5 0
<br /> tert-Bury]benzene ND<10 10 5 0 Methyl ethyl ketone ND<10 20 10
<br /> Carbon Disulfide ND<10 10 5 0 Methyl isoburyl ketone a ND<10 1 0 50
<br /> Carbon Tetrachloride ND<10 10 5 0 Methyl tert-Butyl Ether(MTBE) 10 5 0
<br /> Chlorobenzene ND<10 10 5 0 Naphthalene ND<10 50 50
<br /> Chloroethane ND<10 10 50 n-Propyl benzene 29 10 5 0
<br /> I 2-Chloroethyl Vinyl Ethe ND<10 10 50 Styrene ND<10 10 5 0
<br /> Chloroform ND<10 10 50 1,1,1,2-Tetrachloroethane ND<10 10 50
<br /> Chloromethane ND<10 1 0 50 1,1,2,2-Tetrachloroethane ND<10 10 50
<br /> 2-Chlorotoluene ND<10 10 50 Tetrachloroethene ND<10 10 5 0
<br /> 4-Chlorotoluene ND<10 1 0 50 Toluene 130 10 5 0
<br /> Dibromochloromethane ND<10 10 5 0 12,3-Tnchlorobenzene ND<10 5 0 25
<br /> 1,2-Dibromo-3-chloropmpane ND<10 2 0 10 1,2,4-Trichlorobenzene ND<10 5 0 25
<br /> Dibromomethane ND<10 10 50 1,1,1-Tnchloroethane ND<10 10 5 0
<br /> 1,2-Dichlorobenzene ND<10 10 50 1 1 2-Trich1oroethane 26 10 50
<br /> 1,3-Dichlorobenzene ND<10 10 5 0 Trichloroethene ND<10 10 50
<br /> 114-Dichlorobenzene ND<10 10 50 Trichlorofluoromethane ND<10 10 50
<br /> Dichlorodifluoromethane ND<10 10 50 1,2,3-Tncbloropropane ND<10 10 50
<br /> l,l-Dichloroethane ND<10 10 5 0 1,2,4-Tnmethylbenzene 100 10 50
<br /> 1,2-Dichloroethane ND<10 10 50 1,3,5-Tnmethylbenzene 29 1 0 5 0
<br /> I,1-Dichloroethene ND<10 1 0 5 0 Vinyl Acetate '° ND<10 5 0 25
<br /> cis-1 2-Dichloroethene ND<10 10 5 0 Vinyl Chlunde ° ND<10 10 50
<br /> trans-1,2-Dichloroethene ND<10 10 50 Xylenes,total 250 10 50
<br /> 1,2-Ihchloropropane ND<10 10 5 0 Comments
<br /> I,3-Dichloropropane ND<10 10 5 0 Surrogate Recoveries(%)
<br /> Y2-Dichloropropane ND<10 10 50 Dibromofluoromethane 114
<br /> 1,1-Dichlomp opene NIK10 10 5 0 Toluene-d8 105
<br /> cis-1,3-Dichloropropene N13<10 10 50 4-13mmofluornbenzene 103
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts m ug/L
<br /> ND means not detected above the reporting lirrat,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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