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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//wwwmecampbellcom E-mail main@mccampbell com
<br /> Advanced GeoEnvironinental Client Project ID K& S Gas &Grocery Date Sampled 02/14/01 II
<br /> 837 Shaw Road Date Received 02/20/01
<br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/20/01
<br /> Client P O Date Analyzed 02121-02128101
<br /> Volatile Organics By GUMS
<br /> EPA method 8260
<br /> Lab ID 60460
<br /> Client ID P-2171-72'
<br /> Matrix S
<br /> Rzporng Limit Rcpormig Limit
<br /> Compound Concentration* wUS Compound Concentration* w S
<br /> Acetone(b) ND 5 0 25 bans-1,3-Dichloropropene ND 10 50
<br /> Benzene 5 4 1 0 5 0 Ethylene dibromide ND 10 50
<br /> Bromobenzene ND 1 0 5 0 Ethylbenzene ND 10 5 0
<br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 5 0
<br /> Bromoform ND 1 0 5 0 Isopropylbenzenc ND 10 5 0
<br /> Bromomethane ND 10 5 0 p-Isopropyl toluene ND 10 5 0
<br /> I n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 10 5 0 Methylene Chloride(') ND 10 50
<br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketone ND 10 5 0
<br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) -- 10 50
<br /> Chlorobenzene ND 10 5 0 Naphthalene ND 5 0 5 0
<br /> Chloroethane ND 1 0 5 0 n-Propyl benzene ND 10 5 0
<br /> 2-Chloroethyl Vinyl Ether` ND 1 0 50 Styrene Iml ND 1 0 50
<br />' Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND 10 5 0
<br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 10 5 0
<br /> I 4-Chlorotoluene ND 1 0 50 Toluene ND 10 50
<br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 5 0 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 5 0 25
<br /> Dibromomethane ND 1 0 5 0 1,1,1-Tnchloroethane ND 10 5 0
<br /> I 1 2-Dichlorobenzene ND 1 0 50 1 1,2-Tnchloroethane ND 10 5 0
<br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 10 50
<br /> Dichlorodifluoromethane ND 1 0 50 1,2 3-Tnchloropropane ND 1 0 5 0
<br /> 1,I-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichloroethane ND 1 0 50 1,3,5-Trimethylbenzene ND 1 0 50
<br /> 1,I-Dichloroethene ND 1 0 50 Vinyl Acetate m ND 5 0 25
<br /> cis-1,2-13icliloroethene ND 10 5 0 Vinyl Chloride ° ND 10 5 0
<br /> trans-1 2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane ND 1 0 5 0 Comments
<br /> 17achloropropane ND 1 0 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 1 0Dibromofluoromethane 11 i
<br /> 1,1-INchloropropene ND 1 0Toluene-dg 109
<br /> cis-1,3-Dichloropropene ND lot4-Bromofluorobenzene 114
<br /> water and vapor samples are reported in ug/L soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlomethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (0 2-butanone (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water rnuruscible sheen is present, (i)liquid sample that contains greater than—5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (I methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton,Lab Director
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