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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbellcom E-mail main@mecampbell corn <br /> Advanced GeoEnvironmental Client Project ID K& S Gas &Grocery Date Sampled 02/14/01 <br />' 837 Shaw Road <br /> Date Received 02/20/01 <br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01 <br />' Client P O Date Analyzed 02/21-02/28/01 <br /> Volatile Organics By GC/MS <br /> BPA method 8260 <br />' Lab ID 60459 <br /> Client ID P-2/93` <br /> Matrix W <br /> Reporting Limit Compound <br /> Lima <br />' Compound Concentration* W S Compound Concentration* S <br /> Acetone ro ND 50 25 trans-1,3-Dichloropropene ND —T—o 5o <br /> Benzene 32 10 50 Ethylene dibromide ND 10 50 <br />' Bromobenzcm ND 10 5 0 Ethylbenzene ND 10 5 0 <br /> Bromochloromethane ND 10 5 0 1 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 5 0 lodomethane ND 10 5 0 <br /> Bromoform ND 1 0 5 0 lsopropylbenzene ND 10 5 0 <br />' Bronwmethane ND 10 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND 10 50 <br /> tent-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND to 50 Methyl isobutyl ketone R ND to 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) 10 5 0 <br /> Chlorobenzene ND 10 5 0 Naphthalene ND 50 50 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 5 0 <br />' 2-Chloroethyl Vinyl hther'ei ND 10 50 Styrene ND 10 5 0 <br /> Chloroform ND 10 50 1 1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 5 0 1,1,2,2-Tetrachloroethane ND lo 5 0 <br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethene ND 10 5 0 <br />' 4-Chlorotoluene ND 10 50 Toluene ND 10 5 0 <br /> Dibromochloromethane ND to 50 1,2,3-Tnchlombenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Trichlorobenzene ND 50 25 <br /> Dibromonothane ND 10 50 1,1,1-Tnchloroethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dieblorobenzene ND 1 0 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 10 50 <br />' 1,1-Dichloroethane ND 1 0 50 t,2,4-Trimethylbenzene ND 10 5 0 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 10 50 <br /> 11-Dichloroethene ND 1 0 5 0 Vinyl Acetate '° ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride ND 1 0 5 0 <br />' trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 10 5 0 Surrogate Recoveries{%) <br /> 2,2-Dichloropropane ND 10 5 0 Dibromofluoromethane 119 <br />' 1,1-Dichloropropene ND 10 50 Toluene-d8 103 <br /> cis-1,3-I31chloropropene ND 1 0 5 0 4-Bromofluorobenzene 100 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content, (c) ethenylbenzene, 0? methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />