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<br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> titin//www mccampbell corn F-marl mom@mccampbeil cam
<br />' Advanced GeoEnvironmental Client Protect M K&S Gas&Grocery Date Sampled 02/14/01
<br /> 837 Shaw Road Date Received 02/20/01
<br /> IStockton,CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01
<br /> Client P O Date Analyzed 02/21-02128/01
<br />' Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab 1D 60462
<br /> Client 1D P-3/55-60'
<br /> Matrix W
<br /> Compound Concentration* Rcpamng Lunt Compound Concentration Rcpartmg Lmnt
<br />' W S W S
<br /> Acetone rni ND<20 50 25 trans-1,3-Dichloropropene NIK20 10 5 0
<br /> Benzene 740 1 0 5 0 Ethylene dibromide NIK20 10 5 0
<br />' 13mmobenzene ND<20 10 5 0 Ethylbenzene 73 10 50
<br /> Bromochloromethane ND<20 10 50 Hexachlorobutadiene ND<20 5 0 25
<br /> Bromodiehloromethane ND<20 10 50 Iodomethane N1K20 10 50
<br /> Bromoforni ND<20 10 5 0 Iscpivpylbenzene 22 10 5 0
<br />' Bromomethane ND<20 10 50 p-Isopropyl toluene ND ,20 10 5 0
<br /> n-Butyl benzene NIK20 10 5 0 Methyl butyl ketone NIK20 10 5 0
<br /> sec-Butyl benzene ND<20 10 5 0 Methylene Chloride(') ND<20 10 50
<br /> tert-Butyl benzene ND<20 10 5 0 Methyl ethyl ketone ND<20 2 0 10
<br /> Carbon Disulfide ND<20 10 50 Methyl isobutyl ketones ND<20 10 5 0
<br /> Carbon Tetrachloride ND<20 10 5 0 Methyl tort-Butyl)ether(MTBE) 10 5 0
<br /> Chlorobenzene ND<20 10 5 0 Naphthalene ND<20 5 0 5 0
<br /> Chloroethanc ND<20 1 0 5 0 n-Propyl benzene 74 10 5 0
<br />' 2-Chloroethyl Vinyl Ether" ND<20 1 0 5 0 Styrene ND<20 10 5 0
<br /> Chloroform ND<20 1 0 5 0 1,1,1,2-Tetrachloroethane ND<20 i 1 0 5 0
<br /> Chloromethane ND<20 10 50 1,1,2,2-Tetrachloroethane ND<20 10 5 0
<br /> 2-Chlorotoluene ND<20 1 0 5 0 Tetrachloroethene ND<20 10 5 0
<br />' 4-Chlorotoluene ND<20 1 0 5 0 Toluene ND<20 10 5 0
<br /> Dibromochloromethane ND<20 1 0 5 0 1,2,3-Tnehlorobenzene NIK20 50 25
<br /> 1,2-Dibromo-3-chloropropane NIK20 2 0 10 1,2,4-Tnchlorobenzene ND<20 5 0 25
<br /> Dibromomethane ND<20 1 0 5 0 1,1,1-Tnchloroethane ND<20 1 0 5 0
<br />' 1,2-Dichlorobenzene ND<20 1 0 5 0 1,1,2-Tnchloroethane 30 1 0 5 0
<br /> 1,3-Dichlorobenzene ND<20 1 0 5 0 Trichloroethene ND<20 1 0 5 0
<br /> 1,4-Dichlorobenzene ND<20 1 0 5 0 Tnchlorofluoromethane ND<20 1 0 5 0
<br /> Dichlorodifluoromethane ND<20 1 0 5 0 1,2,3-Tnchloropropane ND<20 1 0 5 0
<br />' 1,1-Dichloroethane ND<20 10 50 1,2,4-Tnmethylbenzene ND<20 10 50
<br /> 1,2-Dichloroethane ND<20 1 0 5 0 1,3,5-Trimethylbenzene ND<20 10 5 0
<br /> l,t-Dichloroethene ND<20 1 0 5 0 Vinyl Acetate m ND<20 5 0 25
<br /> cis-1,2-D ehloroethene ND<20 1 0 5 0 Vinyl Chloride " ND<20 10 5 0
<br />' trans-l,2-Dichloroethene ND<20 1 0 5 0 Xylenes,total 31 to 5 0
<br /> 1,2-Dichloropropane ND<20 1 0 5 0 Comments
<br /> 1,3-Dichloropropane ND<20 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND<20 1 0 5 0 Dibromofluoromethane 117
<br />' 1,1-Dichloropropene ND<20 10 50 Toluene-d8 104
<br /> cis-1,3-Dichloropropane ND<20 10 __50 4-Bromofluorobenzene 102
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlomethoxy) ethene, (d) 2-bexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i) liquid sample that contains greater than -5 vol %
<br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chioroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamiiton,Lab Director
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