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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> McCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbell corn E-mail mamQmccampbell corn
<br />' Advanced GeoEnvironmental Client Project ID K& S Gas &Grocery Date Sampled 02/14/01
<br /> :Ir
<br /> 837 Shaw Road Date Received 02/20/01
<br />' Stockton,CA 95215 Client Contact Calvin Lee Date Extracted 02121-02/28/01
<br /> Client P O Date Analyzed 02/21-02/28/01
<br />' Volatile Organics By GC/MS
<br /> EPA method 8260
<br />' Lab ID 60463
<br /> Client ID P-3177-81'
<br /> Matrix W
<br /> * Rcportmg Li=t * RcpoMng Limit
<br />' Compound Concentration W $ Compound Concentration* W S
<br /> Acetone mi ND 50 25 trans-l,3-Dchlaropropene ND 10 50
<br /> Benzene ND 10 50 Ethylene dibromide ND 10 50
<br /> Brornobenzene ND 10 50 Ethylbenzene ND 10 so
<br />' Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25
<br /> Bromodichloromethane ND 10 50 iodomethane ND 10 so
<br /> Bromofonn ND 10 50 Isopropylbenzene ND 10 so
<br />' Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 50
<br /> n-Butyl benzene ND 10 J 50 Methyl butyl ketone ND 10 50
<br /> sec-Butyl benzene ND 1 0 1 50 Methylene Chlondel'3 ND 1 0 50
<br /> tert-Butyl benzene ND 1 0 50 Metbyl ethyl ketone ND 20 10
<br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND 10 50
<br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) 10 50
<br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 50
<br /> Chloroethane ND 10 50 n-Propyl benzene ND to 50
<br />' 2-Chloroethyl Vinyl Ether") ND 10 50 Styrene ND 1 0 50
<br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50
<br /> Chloromethane ND 10 50 1,1,22-Tetrachloroethane ND 10 50
<br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 1 0 50
<br />' 4-Chlorotoluene ND 10 50 Toluene ND 10 50
<br /> Dibromochloromethane ND 10 50 1,2,3-Tnehlorobenzene ND 50 25
<br /> 12-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 10 50
<br />' 1,2-Dichlorobenzene ND 10 50 1,1,2-Trichloroethane ND 10 50
<br /> 1,3-Dichlorobenzene ND l 0 50 Trichloroethene ND 10 50
<br /> 14-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 50
<br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchloropropane ND 10 50
<br />' 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50
<br /> 1,2-Dichlomethane ND 10 50 1,3,5-Tnmethylbenzene ND 10 50
<br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate") ND 50 25
<br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride ND 10 50
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<br /> trans-l,2-Dichloroethene ND to 50 Xylenes,total ND 10 50
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 119
<br /> I 1,1-Dichloropropene ND 1 0 50 Toluene-d8 105
<br /> cis-1,3-Dichloroptropene ND 1 0 50 4-Bromofluorobenzene 102
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L,
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (t)liquid sample that contains greater than --5 vol %
<br /> Sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 JEA Edward Hamilton,Lab Director
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