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I <br /> 110 2nd Avenue South,##137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http!/www mccampbell corn E-mail main@mccampbell corn <br /> IAdvanced GeoEnvironmentai Client Project ID K& S Gas& Grocery Date Sampled 02/14/01 l <br />' 837 Shaw Road <br /> Date Received 02/20/01 <br /> Stockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01 <br />' Client P O Date Analyzed 02/21-02/28/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 60465 <br /> P-3/117- Reporting Limit <br /> Client ID 121' <br />' Matnx W --- S w <br /> Compound Concentration* ug/kg ug/L <br /> IDi-isopropyl Ether(D1PE) ND<5 0 50 10 <br />' Ethyl tert-Butyl Ether(ETBE) ND<5 0 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) ND<5 0 50 <br /> 10 <br /> tent-Amyl Methyl Ether(TAME) ND<5 0 50 1 0 <br /> tert-Butanol ND<25 25 so <br /> IMethanol ND<1000 1000 200 <br /> Ethanol ND<250 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluorometbane 117 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting lirmt,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water inumscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0}sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />