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I <br /> 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> 4 MCCA.WBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hgR//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvtronmental Client Project ID K&S Gas& Grocery Date Sampled 02/14/01 V <br /> 837 Shaw Road Date Received 02/20/01 <br /> IStockton, CA 95215 Client Contact Calvin Lee Date Extracted 02/21-02/28/01 <br />' Client P O Date Analyzed 02/21-02/28/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 60461 60462 60463 60464 <br /> Reporting Lirnit <br /> Client ID P-3/30-40' P-3155-60' P-3/77-81' P-3/95-97' <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND<20 ND ND 50 10 <br /> I Ethyl tert-Butyl Ether(ETBE) ND ND<20 ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND ND<20 ND ND so 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND<20 ND ND 50 1 0 <br /> tert-Butanol ND ND<100 ND ND 25 50 <br /> Methanol ND ND<4000 ND ND 1000 200 <br /> Ethanol ND ND<1000 ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 118 117 119 118 <br /> Comments <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water inuriiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />