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ICastle Analytical Laboratory, Atwater, CA <br /> Lab Report No H5041903 Date 04/27/2005 Page 8 <br /> Protect Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Project No N/A Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-4 Lab Samp ID 8016-4W <br /> Descr/Location MW-4 Recd Date 04/19/2005 <br /> Sample Date 04/18/2005 Prep Date 04/21/2005 <br /> Sample Time 1410 Analysis Date 04/21/2005 <br /> Matrix Water QC Batch VWMS-4215 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Did <br /> Methyl-tert-butyl ether(MTBE) 0289 05 MRL 21 UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 0 084 05 MRL ND UG/L 1 <br /> I tert-Amyl methyl ether(TAME) 0 067 05 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0155 05 MRL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 879 20 MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0 081 05 MRL 75 UG/L 1 <br /> 1,2-Dibromoethane 0 092 05 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> Toluene-d8 63-132 SLSA 961% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 954% 1 <br /> I� <br /> "� y5 <br /> Approved by 4J ` .� r __ Date 2 <br />