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Castle Analytical Laboratory, Atwater, CA <br /> ILab Report No H5041903 Date 04/27/2005 Page 9 <br /> Protect Name BENETO TANK LINES#8 Analysis Volatile Organic Compounds by GC/MS Fuel <br />' Protect No NIA Method $280FA <br /> Prep Meth SW5030B <br /> I Field ID MW-5 Lab Samp ID 8016-5W <br /> Descr/Location MW-5 Rec'd Date 04/19/2005 <br /> Sample Date 04/18/2005 Prep Date 04/21/2005 <br /> Sample Time 1542 Analysis Date 04/21/2005 <br /> Matnx Water OC Batch VWMS-4215 <br /> Basis Not Filtered Notes DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0 578 1 MRL 27 UGIL 2 <br /> Ethyl tert-butyl ether(ETBE) 0168 1 MRL ND UGIL 2 <br /> I Cert-Amyl methyl ether(TAME) 0134 1 MRL ND UGIL 2 <br /> Di-isopropyl ether(DIPE) 031 1 MRL ND UGlL 2 <br /> tert-Butyl alcohol (TBA) 1758 40 MRL 62 UG/L 2 <br /> I 1,2-Dichloroethane 0 162 1 MRL 25 UG/L 2 <br /> 1,2-Dibromoethane 0184 1 MRL ND UGIL 2 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br />' Toluene-d8 63-132 SLSA 671% 1 <br /> 1,2-Dichloroethane-d4 59-135 SLSA 841% 1 <br /> AwL Dl= Reporting limits elevated due to matnx interferences <br /> i <br /> I <br /> I <br /> 1 <br /> Approved by `� _ Date �� ? 71 UJB <br />