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According to the California Code of Regulation (CCR), a waste is toxic if it contains lead <br />above 1,000 mg/kg (its Total Threshold Limit Concentration or TTLC) or if it could produce <br />a leachate above its Soluble Threshold Limit Concentration (STLC) of 5.0 milligrams per liter <br />(mg/1). None of the samples exceeded 1,000 mg/kg lead. <br />However, if the reported lead concentration in a soil sample is numerically greater than ten <br />times the STLC, a Toxic Characteristic Leaching Procedure (TCLP) and a Waste Extraction <br />Test (WET or STLC test) are required to see if the sample is able to produce a leachate with <br />a concentration greater than the STLC. The reported concentrations in D2 (153 mg/kg) and <br />D3 (177 mg/kg) were above 10 times the STLC (50 mg/kg), so additional testing was <br />conducted. <br />The TCLP is used to determine if a waste is toxic under the federal Resource Conservation <br />and Recovery Act (RCRA). The TCLP procedure uses 20 milliliters (ml) of acetic acid per <br />gram of sample to extract the lead into solution over 18 hours, and the solution is then <br />analyzed. The TCLP results were 0.82 mg/I for D2, and less than 0.1 mg/I for D3. <br />The WET is used to determine if a waste is toxic under the CCR. The WET uses 10 ml of <br />citric acid per gram of sample to extract the lead into solution over 48 hours, and the <br />solution is then analyzed. The WET results were 11.1 mg/I for D2 and 5.2 mg/I for D3. <br />Based on analytical results, samples D2 and D3 were determined to be toxic under CCR, <br />but not under RCRA. They are considered to be California hazardous, non-RCRA wastes. <br />Remedial Excavations <br />On December 13, 2007, with the concurrence of Mr. Nuel Henderson of the SJEHD, TLM <br />dug two 4 -foot deep, sloped excavations (Figure 2) to remove the toxic soil. An <br />approximately 2 -foot by 4 -foot excavation was dug beneath D2, and an approximately 2 - <br />foot by 3 -foot excavation was dug beneath D3. Soil samples were collected under your <br />supervision at the bottom of each excavation at approximately 4 feet bg using the hand <br />auger, and on the walls in the ordinal directions at approximately 3.5 feet bg by hand. <br />Excavated soils were containerized in two 55 -gallon drums to await disposal. The <br />excavations were backfilled with gravel. <br />The ten soil samples were analyzed for total lead using U.S. EPA 6010. Two of the samples <br />contained lead above 50 mg/kg: D2-3.5' S (56 mg/kg) and D2 -3.5'W (192 mg/kg). WETs <br />were conducted on the two samples, with results of 0.5 mg/I and 3.6 mg/l, respectively. <br />Soil Disposal <br />On December 28, 2007, the two drums were removed from the site for transport to US <br />Ecology in Beatty, Nevada, for disposed of as California hazardous, non-RCRA hazardous, <br />waste. The uniform hazardous waste manifest is attached. <br />071001/TLM Stockton Report.doc 3 <br />January 29, 2008 " VA P P S <br />