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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC. Telephone :925-798-1620 Fax:925-798-1622 <br /> http://www.mccampbell.com E-mail: main@mccampbell.com <br /> ' Advanced GeoEnvironmental Client Project ID: Hess Du Bois Date Sampled:04/18-04/19/01 <br /> 837 Shaw Road Date Received:04/23/01 <br /> ' Stockton,CA 95215 Client Contact: Bill Little Date Extracted: 04/23/01 <br /> ' Client P.O: Date Analyzed: 04/23-04/26/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 65983 <br /> ' Client ID MW8-40 <br /> Matrix S <br /> Reporting Limit Reporting Limit <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone(b! ND 5.0 25 trans-l,3-Dichloropropene ND IA 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND Lo 5.0 <br /> Bromobenzene ND 1.0 5.0 Hthylbenzene ND 1.0 5.0 <br /> ' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ADD 1.0 5.0 fodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> ' n-Butyl benzene AID 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 t0 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) -- 1.0 5.0 <br /> Chlombenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether" ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> ' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachiomethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4=Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> ' 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorolluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND L.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND L.0 5.0 <br /> IJ-Dichloroethene ND 1.0 5.0 Vinyl Acetate 11 ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> ' trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND L0 5A Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND L0 5.0 Dibromofluoromethane 114 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 101 <br /> cis-1,3-Dichloropropene ND 1.0 1 5.0 4-Bromofluorobenzene 113 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> ' (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d)2-hexanone, (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol. % <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />