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1 <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC; Telephone:925-798-1620 Fax:925-798-1622 <br /> littp://www.mecampbell.com E-mail:main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID:Hess Du Bois Date Sampled: 04/18.04/19/01 <br /> 837 Shaw Road Date Received: 04/23/01 <br /> Stockton,CA 95215 Client Contact: Bill Little Date Extracted:04/23/01 <br /> Client P.O: Date Analyzed:04/23-04/26/01 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 65984 <br /> ' Client ID MW8-45 <br /> Matrix S <br /> Rcpmting Limit Reporting Limit <br /> Compound Concentration* Compound Concentration* <br /> Acetone(b) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> ' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 1 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> n-Butyi benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> ' sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 SA Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketones ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tea-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND S.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> 2-Chloroethyl Vinyl_Eth_,TcT ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> ' Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND t.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> ' 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromcthane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> ' 1,2-Dichloroetbane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> l,l-Dichloroethene ND i.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichlomethene ND 1.0 5.0 Vinyl Chloride ND 1.0 5.0 <br /> trans-l,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichlompropane ND LO 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 113 <br /> ' 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 99 <br /> c7is4,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene In <br /> 'water and vapor samples are reported in ug/1„soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not dctected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; p) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 dward Hamilton,Lab Director <br />