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1 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 McCAMPBELL ANALYTICAL INC. Telephone;925-798-1620 Fax:925-798-1622 http://www.mgg.gn bell.com E-mail:main@mccampbell.com 1 Advanced GeoEnvironmental Client Project ID:Hess Du Bois Date.Sampled: 04/18-04/19/01 837 Shaw Road Date Received: 04/23/01 1 Stockton, CA 95215 Client Contact: Bill Little Date Extracted:04/23/01 Client P.O: Date Analyzed:04/23-04/26/01 Volatile Organics By GUMS EPA method 8260 Lab ID 65987 Client ID MW9-40 Matrix S Reporting Limit ReNniog Limit ' Compound Concentration* W S Compound Concentration* W S Acetone(b) ND<25,000 5.0 25 trans-0-Dichloropropene ND<1000 1.0 5.0 Benzene ND<1000 1.0 5.0 Ethylene dibromide ND<1000 1.0 5.0 ' Bromobenzene ND<1000 1.0 5.0 Ethylbenzene ND<1000 1.0 5.0 Bromochloromethane ND<1000 1.0 5.0 Hexachlorobutadiene ND<1000 5.0 25 Bromodichloromethane ND<1000 1.0 5.0 lodomethane ND<1000 1.0 5.0 Bromoform ND<1000 1.0 5.0 Isopropylbenzene 1200 1.0 5.0 ' Bromomethane ND<1000 l.0 5.0 p-Isopropyl toluene ND<1000 1.0 5.0 n-Butyl benzene 5600 1.0 5.0 Methyl butyl ketone cel ND<1000 1.0 5.0 sec-Butyl benzene 3400 1.0 5.0 Methylene Chloride(`) ND<4500 1.0 5.0 tert-Bu I benzene ND<1000 LO 5.0 Methyl ethyl ketone 1° ND<1000 2.0 10 M Carbon Disulfide ND<1000 1,0 5.0 Methyl isobutyl ketone ND<1000 1.0 5.0 Carbon Tetrachloride ND<1000 1.0 5.0 Meth 1 tert-Bu I Ether(MTBE) 1.0 5.0 Chlorobenzene ND<1000 1.0 5.0 Na hthalene 2100 5.0 5.0 Chloroethane ND<1000 1.0 5.0 n-Propyl benzene 4500 1.0 5.0 ' 2-Chloroethyl Vinyl Ethert`) ND<1000 1.0 5.0 Styrene('. ND<1000 1.0 5.0 Chloroform ND<1000 1.0 5.0 1,1,1,2-Tetrachloroethane ND<1000 1.0 5.0 Chloromethane ND<1000 1.0 5.0 1,1,2,2-Tetrachloroethane ND<1000 1.0 5.0 -_ 2-Chlorotoluene - - -- ND<1000 1.0 5.0 Tetrachloroethene ND<1000 1.0 5.0 4-Chlorotoluene ND<1000 1.0 5.0 Toluene() ND<1000 1.0 5.0 Dibromochloromethane ND<1000 1.0 5.0 1,2,3-Trichlorobenzene ND<1000 5.0 25 1,2-Dibromo-3-chloropropane ND<1000 2.0 t0 1,2,4-Trichlorobenzene ND<1000 5.0 25 Dibromomethane ND<1000 1.0 5.0 1,1,1-Trichloroethane ND<1000 1.0 5.0 1,2-Dichlorobenzene ND<1000 1.0 5.0 1,1,2-Trichloroethane ND<1000 1.0 5.0 1,3=Dichlorobenzene ND<1000 1.0 5.0 Trichloroethene ND<1000 1.0 5.0 1,4-Dichlor0benzene ND<1000 1.0 5.0 Trichlorofluoromethane ND<1000 1.0 5.0 Dichlorodifluoromethane ND<1000 1.0 5.0 1,2,3-Trichloropropane ND<1000 1,0 5.0 ' 1,1-Dichloroethane ND<1000 L0 5,0 1,2,4-Trimethylbenzene ND<1000 LO 5.0 1,2-Dichloroethane ND<1000 1.0 5.0 1,3,5-Trimeth lbenzene ND<1000 1.0 5.0 [,I-Dichloroethene ND<1000 L0 5.0 Vinyl Acetate(n) ND<1000 5.0 25 cis-1,2-Dichloroethene ND<1000 L0 5.0 Vinyl Chloride ND<1000 1.0 5.0 ' trans-l,2-Dichloroethene ND<1000 1.0 5.0 Xylenes,total ND<1000 1,2-Dichloropropane ND<1000 1.0 5.0 Comments: 1,3-Dichloro ro ane ND<1000 1.0 5.0 Surrogate Recoveries 2,2-Dichloropropane ND<1000 1.0 5.0 Dibromofluoromethane 104 ' l,l-Dichloropropene ND<1000 1.0 5.0 Toluene-d8 103 cis-1,3-Dichlororo ene ND<1000 1.0 5.0 4-Bromofluorobenzene 96 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L ' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than-5 vol. % sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) ' chloroethene; o dimethylbenzenes. DHS Certification No. 1644 Edward Hamilton, Lab Director