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g, 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ® McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://w-ww.mgqgglbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Hess Du Bois Date Sampled: 04/18-04/19/01 <br /> d 1 <br /> 837 Shaw Road Date Received: 04/23/01 <br />' Stockton, CA 95215 Client Contact: Bill Little Date Extracted:04/23/01 <br />' Client P.O: Date Analyzed:04/23-04/26/01 <br /> Volatile Organics By CUMS <br /> EPA method 8260 <br /> ' Lab ID 65986 <br /> Client ID MW9-30 <br /> Matrix S <br /> Rep°rting Limit Reporting Limit <br /> ' Compound Concentration* W S Compound Concentration* W S <br /> Acetone M ND<25,000 5,0 25 trans-1,3-Dichloropropene ND<1000 LO 5.0 <br /> Benzene ND<1000 l.0 5.0 Ethylene dibromide ND<t000 1.0 5.0 <br /> Bromobenzene ND<1000 1.0 5.0 Ethylbenzene ND<1000 1.0 5.0 <br /> ' Bromochloromethane ND<]000 1,0 5.0 Hexachlorobutadiene ND<1000 5.0 25 <br /> Bromodichloromethane ND<1000 1.0 5.0 lodomethane ND<1000 CO- 5.0 <br /> Bromoform ND<1000 L0 5.0 Iso rop lbenzene ND<1000 1.0 5.0 <br /> ' Bromomethane ND<1000 1.0 5.0 p-Isopropyl toluene ND<1000 1.0 5.0 <br /> n-Butyl benzene 2700 1.0 5.0 Methyl butyl ketone(d) ND<1000 1.0 5.0 <br /> sec-Butyl benzene 2500 1.0 5.0 Methylene Chloride'`' ND<4500 LO 5.0 <br /> tert-Butyl benzene ND<1000 1.0 5.0 Methyl ethyl ketoneND<1000 2.0 10 <br /> M Carbon Disulfide ND<1000 1.0 5.0 Methyl isobutyl ketone ND<1000 1.0 5.0 <br /> Carbon Tetrachloride ND<1000 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND<L000 1.0 5.0 Naphthalene 1500 5.0 5.0 <br /> Chloroethane ND<1000 1.0 5.0 n-Propyl benzene 3400 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether`) ND<1000 1.0 5.0 Styrene M ND<1000 1.0 5.0 <br /> ' Chloroform ND<1000 1.0 5.0 1,1,1,2-Tetrachloroethane ND<1000 1.0 5.0 <br /> Chloromethane ND<1000 1.0 5.0 1,1,2,2-Tetrachloroethane N13<1000 1.0 5.0 <br /> 2=Chlorotoluene" ND<1000 1.0 -5.0 Tetrachloroethene ND<1000 -Lo - 5.0 -- <br /> ' 4-Chlorotoluene ND<1000 1.0 5.0 Toluene"' ND<1000 1.0 5.0 <br /> Dibrornochloromethane ND<1000 1.0 5.0 1,2,3-Trichlorobenzene ND<1000 5.0 25 <br /> 1,2-Dibromo-3�hloropropane ND<1000 2.0 10 1,2,4-Trichlorobenzene ND<1000 5.0 25 <br /> Dibromomethane ND<1000 1.0 5.0 1,1,1-Trichloroethane ND<1000 1.0 5.0 <br /> ' 1,2-Dichlorobenzene ND<1000 1.0 5.0 1,1,2-Trichloroethane ND<1000 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<1000 1.0 5.0 Trichloroethene ND<1000 1.0 .5.0 <br /> 1,4-Dichlorobenzene ND<1000 1.0 5.0 Trichlorofluoromethane ND<1000 1.0 5.0 <br /> Dichlorodifluoromethane ND<1000 1.0 5.0 1,2,3-Trichloropropane N13<1000 1.0 5.0 <br /> ' 1,1-1)ichloroethane ND<1000 1.0 5.0 1,2,4-Trimeth lbenzene ND<1000 L0 5.0 <br /> 1,2-Dichloroethane ND<1000 1.0 5.0 1,3,5-Trimethylbenzene ND<1000 1.0 5.0 <br /> I,1-Dichloroethene ND<1000 1.0 5.0 Vinyl AcetateW ND<1000 5.0 25 <br /> cis-1,2-Dichloroethene ND<1000 L0 5.0 Vinyl Chloride N13<1000 1.0 5.0 <br /> ' trans-1,2-Dichloroethene ND<1000 1.0 5.0 Xylenes,total <br /> 1,2-Dichloropropane ND<1000 1.0 5.0 Comments: <br /> 1,3-Dichloro ro ane ND<1000 1.0 5.0 Surrogate Recoveries <br /> 2,2-Dichloropropane ND<1000 1.0 5.0 Dibromofluoromethane 112 <br /> 1,1-Dichlororopene N13<1000 1.D 5.0 Toluene-d8 106 <br /> cis-1,3-Dichloro ro ene ND<1000 1.0 1 5.0 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SPLP extracts in ug/L' <br /> ' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropyl acetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene; o dimethylbenzenes. 11 <br /> DHS Certification No. 1644 JAId W Edward Hamilton,Lab Director <br />