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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ,ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> ' http://www.mccampbell.com E-mail:main@mccampbcll.com <br /> Advanced GeoEnvironmental Client Project ID: Hess Dubois Date Sampled: 12/22/00 <br /> 4005 North Wilson Way Date Received: 12/27/00 <br /> ' Stockton,CA 95205 Client Contact:William Little Date Extracted: 12127-01/03/01 <br /> ' Client P.O: Date Analyzed: 12/27-01/03/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> ' Lab ID 56947 <br /> Client ID MW-1112-22-00 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br /> W S W S <br /> Acetone ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> ' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 lsopropylbenzene ND 1.0 5.0 <br /> ' Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride") ND<5.0 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> ' Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> ' 2-Chloroethyl Vinyl Ethe ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chiorotoluene ND 1.0 5.0 Tctrachloroethene ND<5.0 1.0 5.0 <br /> 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-TTichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND LO 5.0 <br /> ' 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate "` ND 5.0 25 <br /> cis-1,2-Dichlotoethene ND 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> trans-l,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropmpane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries{%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluommethane 109 <br /> 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 ]OF- <br /> cis-1,3-Dichloropropene <br /> Olcis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluombenzene 92 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPI.P extracts in ug/L <br /> ND means not detected above the.reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy)ethene;(d)2-hexanone; (e)dichloromethane; (f)2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />