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10 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> hgp://www.mccami)bell.com E-mail:main@tnecampbell.com <br /> Advanced GeoEnyironmental Client Project ID:Hess Dubois Date Sampled: 12/22/00 <br /> 4005 North Wilson Way Date Received: 12/27/00 <br /> Stockton,CA 95205 Client Contact: William Little Date Extracted: 12/27-01103/01 <br /> Client P.O: Date Analyzed: 12/27-01/03/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> ' Lab ID 56948 <br /> Client ID MW-2/12-22-00 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br /> W S W S <br /> Acetone NO 5.0 25 trans-1,3-Dichloropropene NO 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide NO 1.0 5A <br /> ' Bromobenzene NO 1.0 5.0 Ethylbenzene NO 1.0 5.0 <br /> Bromochloromethane NO 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 1 lodometbane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene NO 1.0 5.0 <br /> ' <br /> sec-Butyl <br /> romomethane ND 1.0 5.0 p4sopropyl toluene ND 1.0 5.0 <br /> Butyl benzene NA 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> benzene 3.7 1.0 5.0 Methylene Chloride` ND<5.0 1.0 5.0 <br /> ten-Butyl benzene 1.6 1.0 5.0 Methyl ethyl ketone NO 2.0 10 <br /> ' Carbon Disulfide NO 1.0 5.0 Methyl isobutyl ketone NO 1.0 5.0 <br /> Carbon Tetrachloride NO 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene NO 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene NO 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethe ` ND 1.0 5.0 Styrene M NO 1.0 5.0 <br /> Chloroform. NO 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane NO 1.0 5.0 <br /> 2-Chlorotoluene NO 1.0 5.0 Tetrachloroethene ND<5.0 1.0 5.0 <br /> ' 4-Chlorotoluene NO 1.0 5.0 Toluene 4.1 1.0 5.0 <br /> Dibromochloromethane NO 1.0 5.0 1,2,3-Trichlorobenzene NO 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Triehlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br /> ' 1,2-Dichlorobenzene 2.3 1.0 5.0 1,1,2-Trichloroethane NO 1.0 5.0 <br /> 1,3-Dichlorobenzene NO 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane NO 1.0 5.0 <br /> Dichlorodifluoromethane AIA 1.0 5.0 1,2,3-Trichloropropane NO 1.0 5.0 <br /> 1,1-Dichloroethane NO 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane NO 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> IJ-Dichloroethene NO 1.0 5.0 Vinyl Acetate `° NO 5.0 25 <br /> cis-1,2-Dichloroethene NO 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> ' trans-1,2-Dichloroethene NA 1.0 5.0 Xylenes,total 2.6 1.0 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane NO 1.0 5.0 Dibromofluoromethane 103 <br /> ' 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 97 <br /> cis-1,3-Dichloropropene NO LO 5.0 4-13ramofluorobenzene 93 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' <br /> NO means not detected above the reporting limit;N/A means analyte not applicable.to this analysis <br /> (b) 2-propanone or dimethyl ketone;(c) (2-chloroethoxy)ethene; (d)2-hexanone; (e)dichloromethane; (f)2-butanone; (g)4-methyl-2- <br /> pentanone or isopr6pylacetone; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (l) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene:(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />