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110 2nd Avenue South,#D7,Pacheco;CA 94553-5560 <br /> ' 4 MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> http://www.mccampbell.com E-mail:main@mccatnpbell.com <br /> i .. <br /> Advanced GeoEnviromnental Client Project ID:Hess Dubois Date Sampled: 12/22/00 <br /> 1 4005 North Wilson Way Date Received: 12/27/00 <br /> Stockton, CA 95205 Client Contact: William Little Date Extracted: 12/27-01/03/01 <br /> ' Client Ro: Date Analyzed: 12/27-01/03/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 56950 <br /> Client ID MW4/12-22-00 <br /> Matrix W <br /> * Reporting Limit Reporting Limit <br /> Compound Concentration W 5 Compound Concentration* <br /> W S <br /> Acetone ) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND -1.0 5.0 <br /> ' Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> Bromoehloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> ' Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride` ND<5.0 1.0 5.0 <br /> tert-Butyl benzene ND LO 5.0 Methyl ethyl ketone ND 2.0 10 <br /> ' . Carbon Disulfide ND 1.0 5.0 Mcthyl isobutyl ketone a ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane NO 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br /> ' 2-Chloroethyl Vinyl Eth ND 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene NN <br /> 1.0 5.0 <br /> ' 4-Chlorotoluene ND 1.0 5.0 Toluene 1.0 5.0 <br /> Dibromochloromethanc ND 1.0 5.0 1,2,3-Trichlorobenzene 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene 5.0 25 <br /> Dibromomethane ND lA 5.0 1,1,1-Trichloroethane 1.0 -5.0 <br /> ' 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene 1.4 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br /> ' l,]-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethane ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate ' ND 5.0 25 <br /> cis-1,2-Dichlotoethene 2.1 1.0 5.0 Vinyl Chloride ° ND 1.0 5.0 <br /> trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 5.0 <br /> 1,2-Dichloropmpane ND LO 5.0 Comments: <br /> 1,3-Diehl oropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 107 <br /> ' ],1-Dichloropropene ND 1.0 5.0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 1.6 1 5.0 4-Bromofluorobenzene 03 <br /> water and vapor samples arereported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone;(c)(2-ehloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (0 2-butanonc; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than -5 vol.% <br /> sediment; (j) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification.No. 1644 Edward Hamilton,Lab Director <br />