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r 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 4 MCCANMBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 rkq-://www.mccampbell.com E-mail:mainQa mccampbell-corn • rAdvanced GeoEnvironmental Client Project ID:Hess Dubois Date Sampled: 12/22/00 4005 North Wilson Way Date Received: 12/27/00 rStockton,CA 95205 Client Contact: William Little Date Extracted: 12127-01103101 ' Client P.O: Date Analyzed: 12127-01103101 Volatile Organics By GUMS EPA method 8260 r Lab ID 56949 Client ID MW-3112-22-00 Matrix W Reporting Limit Repotting Limit r Compound Concentration* W S Compound Concentration* W S Acetone 55ND<10 5.0 25 trans-1,3-Dichloropropene ND<10 1.0 5.0 Benzene ND<10 1.0 5.0 Ethylene dibromide ND<10 1.0 5.0 ' Bromobenzene ND<10 1.0 5.0 Ethyibenzene ND<10 1.0 5.0 Bromochloromethane ND<10 1.0 5.0 Hexachlorobutadiene ND<10 5.0 25 Bromodichloromethane ND<10 1.0 5.0 Iodomethane ND<10 1.0 5.0 Bromoform ND<10 1.0 5.0 Isopropylhenzene 54 1.0 5.0 ' Bromomethane ND<10 1.0 5.0 p4sopropyl toluene ND<10 1.0 5.0 n-Butyl benzene ND<10 1.0 5.0 Methyl butyl ketone ND<t0 1.0 5.0 sec-Butyl benzene ND<10 1.0 5.0 Methylene Chloride`O ND<45 1.0 5.0 tent-Butyl benzene ND<10 1.0 5.0 Methyl ethyl ketone ND<10 2.0 10 Carbon Disulfide NIX 10 1.0 5.0 Methyl isobutyl ketone 191 ND<10 1.0 5.0 r Carbon Tetrachloride ND<10 1.0 5.0 Methyl Cert-Butyl Ether(MTBE) --- 1.0 5.0 Chlorobenzene ND<10 1.0 5.0 Naphthalene ND<10 5.0 5.0 Chloroethane ND<10 1.0 5.0 n-Propyl benzene 100 1.0 5.0 ' 2-Cbloroethyl Vinyl Bthe ND<10 1.0 5.0 Styrene ND<10 1.0 5.0 Chloroform ND<10 1.0 5.0 1,1,1,2-Tetrachloroethane ND<10 1.0 5.0 Chloromethane ND<10 1.0 5.0 1,1,2,2-Tetrachloroethane ND<10 1.0 5.0 2-Chlorotoluene ND<10 1.0 5.0 Tetrachloroethene ND<I0 1.0 5.0 ' 4-Chlorotoluene ND<10 1.0 5.0 Toluene ND<10 1.0 -5.0 Dibromochloromethane ND<10 1.0 5.0 1,2,3-Trich1orobenzene ND<10 5.0 25 1,2-Dibromo-3-chloropropane ND<10 2.0 10 1,2,4-Trichlorobenzene ND<10 5.0 25 Dibromomethane ND<10 1.0 5.0 1,1,1-Trichloroethane ND<10 1.0 5.0 r 1,2-Dichlorobenzene ND<10 1.0 S.D 1,1,2-Trichloroethane ND<10 1.0 5.0 1,3-Dichlorobenzene ND<10 1.0 5.0 Trichloroethene ND<10 1.0 5.0 1,4-Dichlorobenzene ND<10 1.0 5.0 Trichlorofluoromethane ND<10 1.0 5,0 Dichlorodifluoromethane ND<10 1.0 5.0 1,2,3-Trichloropropone ND<10 1.0 5.0 r 1,1-Dichloroethane ND<10 1.0 5.0 1,2,4-Trimethylbenzene ND<10 1.0 5.0 1,2-Dichloroethane ND<10 1.0 5.0 1,3,5-Trimethylbenzene ND<10 1.0 5.0 I,1-Dichloroethene ND<10 1.0 5.0 Vinyl Acetate >o ND<10 5.0 25 cis-1,2-Dichloroethene 52 1.0 5.0 Vinyl Chloride " 310 1.0 5.0 r trans-1,2-Dichloroethene ND<10 1.0 5.0 Xylenes,total ND<10 1.0 5.0 1,2-Dichloropropane ND<10 1.0 5.0 Comments: 1,3-Dichloropropane ND<10 1.0 5.0 Surrogate Recoveries(%) 2,2-Dichloropropane ND<10 1.0 5.0 Dibromofluoromethanc 102 r I,1-Dichloropropene ND<10 1.0 5.0 Toluene-d8 100 cis 1,3-Dichlompmpene ND<10 1.05.0 4 Bromofluorabenzene 103 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L r ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis (b)2-propanone or dimethyl ketone; (c) (2-chloroethoxy)ethene;(d)2-hexanone; (e)dichloromethane; (f)2-butanone; (g)4-methyl-2- pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than •-5 vol.% sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) r chloroethene:(o)dimethylbenzenes. DHS Certification No. 1644 Edward Hamilton,Lab Director r