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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax:925-798-1622 - <br /> http://ww_w.mccampbell.com E-mail: main@mccampbell.com <br /> 1 Advanced GeoEnvironmental Client Project ID: Hess Dubois Date Sampled: 12/22/00 <br /> 4005 North Wilson Way Date Received: 12/27/00 <br /> Stockton,CA 95205 Client Contact:William Little Date Extracted: 12127-01103/01 <br /> ' EientP.O: Date Analyzed: 12127-01/03/01 <br /> EPA method 8260 <br /> Volatile Organics By GC/MS <br /> - <br /> ' Lab ID 56952 <br /> Client ID MW-6112-22-00 <br /> Matrix W <br /> Compound Concentration* RcportingLimit * Repw1ingLimit <br /> P W S Compound Concentration W S <br /> ' . Acetone(b5 ND<25 5.0 25 trans-1,3-Dichloropropene ND<25 1.0 5.0 <br /> Benzene ND<25 Lo 5.0 1 Ethylene dibromide ND<25 1.0 5.0 <br /> ' Bromobenzene ND<25 1.0 5.0 Ethylbenzene ND<25 1.0 5.0 <br /> Bromochloromethane ND<25 1.0 5.0 Hexachlorobutadiene ND<25 5.0 25 <br /> Bromodichloromethane ND<25 1.0 5.0 lodomethane ND<25 1.0 5.0 <br /> Bromoform ND<25 1.0 5.0 lsopropylbenzene ND<25 1.0 5.0 <br /> ' Bromomethane ND<25 1.0 5.0 p-Isopropyl toluene ND<25 1.0 5.0 <br /> n-Butyl benzene ND<25 1.0 5.0 Methyl butyl ketone ND<25 1.0 5.0 <br /> sec-Butyl benzene ND<25 1.0 5.0 Methylene Chloride` ND<60 1.0 5.0 <br /> tert-Butyl benzene ND<25 1.0 5.0 Methyl ethyl ketone ND<25 2.0 10 <br /> ' Carbon Disulfide ND<25 1.0 5.0 Methyl isohutyl ketone NIK25 1.0 5.0 <br /> Carbon Tetrachloride ND<25 1.0 5.0 Methyl to t-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND<25 1.0 5.0 Naphthalene ND<25 5.0 5.0 <br /> Chloroethane ND<25 1.0 5.0 n-Propyl benzene ND<25 1.0 5.0 <br /> ' 2-Chloreethyl Vinyl Ether"' ND<25 1.0 5.0 Styrene ND<25 1.0 5.0 <br /> Chloroform ND<25 1.0 5.0 1,1,1,2-Tetrachloroethane ND<25 1.0 5.0 <br /> Chloromethane ND<25 1.0 5.0 1,1,2,2-Tetrachloroethane ND<25 LO 5.0 <br /> 2-Chlorotoluene ND<25 1.0 5.0 Tetrachloroethene 490 1.0 5.0 <br /> ' 4-Chlorotoluene ND<25 110 5.0 Toluene ND<25 1.0 5.0 <br /> Dibromochloromethane ND<25 1.0 5.0 1,2,3-Trichlorobenzene ND<25 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<25 2.0 1 10 1,2,4-Trichloroben7ene ND<25 5.0 25 <br /> Dibromomethane ND<25 1.0 5.0 l,l,l-Trichloroethane ND<25 1.0 5.0 <br /> ' 1,2-Dichlorobenzene ND<25 1.0 5.0 1,1,2-Trichloroethane ND<25 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<25 1.0 5.0 Trichloroethene 460 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<25 1.0 5.0 Trichlorofluoromethane ND<25 1.0 5.0 <br /> Dichlorodifluoromethane ND<25 1.0 5.0 1,2,3-Trichloropropane ND<25 1.0 5.0 <br /> ' 1,1-Dichloroethane ND<25 1.0 5.0 1,2,4-Trimethylbenzene ND<25 1.0 5.0 <br /> 1,2-Dichloroethane ND<25 1.0 5.0 1,3,5-Trimethylbenzene ND<25 1.0 5.0 <br /> 1,1-Dichloroethene ND<25 1.0 5.0 Vinyl Acetate " ND<255.0 25 <br /> cis-1,2-Dichloroethene 1000 1.0 5.0 Vinyl Chloride'"7 220 1.0 5.0 <br /> ' trans-1,2-Dichloroethene ND<25 1.0 5.0 Xylenes,total NIX25 1.0 5.0 <br /> 1,2-Dichloropropane ND<25 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND<25 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichlompropane ND<25 1.D 5.0 Dibromolluoromethane 104 <br /> ' I,l-Dichloropropene ND<25 1.0 5.0 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND<25 1.0 5.0 4-Bromotluorobenzene 512 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c)(2-chloroethoxy)ethene; (d)2-hexanone; (e) dichloromethane; (f)2-butanone; (g)4-methyl-2- <br /> . pentatione or isopropylacetone, (b)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />