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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798.1622 <br /> http://www.mccampbell.com E-mail: main@mccarnpbell.com <br /> Advanced GeoEnvironmental Client Project ID: Hess Dubois .Date Sampled: 12/22/00 <br /> 4005 North Wilson Way Date Received: 12/27/00 <br /> Stockton, CA 95205 Client Contact: William Little Date Extracted: 12/27-01/03/01 <br /> ' Client PA: Date Analyzed: 12/27-01/03/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 56953 <br /> ' Client ID MW-7/12-22-00 <br /> Matrix W <br /> * Repotting Limit Reporting Limit <br /> W S <br /> ' Compound Concentration* Compound Concentration* <br /> W S <br /> Acetone ND<5.0 5.0 25 trans-l,3-Dichloropropene ND<5.0 1.0 5.0 <br /> Benzene ND<5.0 LO 5.0 Ethylene dibromide ND<5.0 1.0 5.0 <br /> Bromobenzene ND<5.0 1.0 5.0 Ethylbenzene ND<5.0 1.0 5.0 <br /> ' Bromochloromethane ND<5.0 1.0 5.0 Hexachlorobutadiene ND<5.0 5.0 25 <br /> Bromodichloromethane ND<5.0 1.0 5.0 todomethane ND<5.0 1.0 5.0 <br /> Bromoform ND<5.0 1.0 5.0 Isopropylbenzene ND<5.0 1.0 5.0 <br /> ' Bromomethane ND<5.0 1.0 5.0 p-Isopropyl toluene ND<5.0 1.0 5.0 <br /> n-Butyl benzene ND<5.0 1.0 5.0 Metbyl butyl ketone ND<5.0 1.0 5.0 <br /> sec-Butyl benzene ND<5.0 1.0 5.0 Methylene Chloride° ND<5.0 1.0 5.0 <br /> tert-Butyl benzene ND<5.0 1.0 5.0 Methyl ethyl ketone ND<5.0 2.0 10 <br /> Carbon Disulfide ND<5.0 1.0 5.0 Methyl isobutyl ketone ND<5,0 1.0 5.0 <br /> ''• Carbon Tetrachloride ND<5.0 1.0 5.0 Methyl tert-Butyl Ether(MTBE) - 1.0 5.0 <br /> Chlorobenzene ND<5.0 1.0 5.0 Naphthalene ND<5.0 5.0 5.0 <br /> Chloroethane ND<5.0 1.0 5.0 n-Propyl benzene ND<5.0 1.0 5.0 <br /> ' 2-Chloroethyl Vinyl Ethe ND<5.0 1.0 5.0 Styrene ND<5.0 1.0 5.0 <br /> Chloroform ND<5.0 1.0 5.0 1,1,1,2-Tetrachloroethane ND<5.0 1.0 5.0 <br /> Chloromethane ND<5.0 1.0 5.0 1,1,2,2-Tetrachloroethane ND<5.0 1.0 5.0 <br /> 2-Chlorotoluene ND<5.0 1.0 5.0 Tetrachloroethene 210 1.0 5.0 <br /> ' 4-Chlorotoluene ND<5.0 1.0 5.0 Toluene 6.0 1.0 5.0 <br /> Dibromochlorornethane ND<5.0 1.0 5.0 1,2,3-Trichlorobenzene ND<5.0 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<5.0 2.0 10 1,2,4-Trichlorobenzene ND<5.0 5.0 25 <br /> Dibromomethane ND<5.0 1.0 5.0 1,1,1-Trichloroethane ND<5.0 1.0 5.0 <br /> ' 1,2-Dichlorobenzene ND<5.0 1.0 5.0 1,1,2-Trichloroethane ND<5.0 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<5.0 1.0 5.0 Trichloroethene 10 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<5.0 1.0 5.0 Trichlorofluoromethane ND<5.0 lA 5.0 <br /> Dichlorodifluoromethane ND<5.0 1.0 5.0 1,2,3-Trichloropropane "-05_0 <br /> 5.0 <br /> ' <br /> IJ-Dichloroethane ND<5.0 1.0 5.0 1,2,4-Trimethylbenzene 5.6 <br /> 1,2-Dichloroethane ND<5.0 1.0 5.0 1,3,5-Trimethylbenzene 5.0 <br /> I,1-Dichloroethene ND<5.0 1.0 5.0 Vinyl Acetate E 25 <br /> cis-l,2-Dichloroethene ND<5.0 1.0 5.0 Vinyl Chloride " 5.0 <br /> trans-l,2-Dichloroethene ND<5.0 LO 5.0 Xylenes,total 5.0 <br /> 1,2-Dichloropropane ND<5.0 LO 5.0 Comments: <br /> 1,3-Dicbioropropane ND<5.0 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<5.0 1.0 5.0 Dibromofluoromethane 105 <br /> ' 1,1-Dichlompropene ND<5.0 1.0 5.0 Toluene-d8 gg <br /> cis-1,3-Dichlompropene ND<5.0 1.0 5.0 4-Bromofluorobenzene 92 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (t)2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than -5 vol.% <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; 0) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />