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26 September 2014 <br /> AGE Project No. 13-2675 <br /> Page 5 of 6 <br /> intrusion. Once vapor wells are set, a two-hour equalization time will be observed prior <br /> to sampling. <br /> One six-liter Summa canister will be utilized for purging and each soil-vapor sample will <br /> be collected in a one-liter Summa canister (TO-15). The sampling and purge canisters <br /> will be connected together with a dedicated and serialized sampling inlet manifold. The <br /> sampling inlet manifold will consist of a vapor-tight valve; a particulate filter; a calibrated <br /> flow restrictor, calibrated to 200 milliliters per minute (ml/min); a stainless steel tee- <br /> fitting; two vacuum gauges at either end of the flow controller and connections for both <br /> purge and sampling canisters (manifold assembly). The manifold assembly will be <br /> attached to the tubing from the temporary/disposable vapor-tips. The purge canister will <br /> be attached to the end of the sampling manifold while the sample canisters will be <br /> attached to the tee-fitting between the tubing and purge container. <br /> Leak tests will be performed on each manifold assembly by attaching and securing the <br /> sample and purge canisters to the manifold and opening the valve on the purge canister <br /> and the manifold. The leak test will be performed for approximately 10 minutes on each <br /> assembly. <br /> Each soil-vapor boring location will be isolated from ambient air by enclosing the <br /> borehole, tubing and manifold/canister assembly in a plastic shroud, which will be <br /> weighted at the surface. Isopropyl alcohol (IPA) as a liquid will be placed in a stainless <br /> steel bowl within the plastic structure and allowed to volatilize into the air enclosed <br /> within the plastic structure surrounding the borehole, tubing and manifold/canister <br /> assembly. <br /> Upon achieving a successful leak test and allowing for 120 minutes of equilibration time, <br /> the purge canister valve will be opened for a calculated period of time to allow for three <br /> calculated volumes of air to be purged. The purge canister vacuum gauge will be <br /> monitored to ensure a proper decrease of vacuum ensuring flow and purging. The <br /> purge volume will be determined by calculating the internal volume of the tubing and <br /> open borehole area (approximately four minutes). <br /> Upon achieving the targeted purge volume, the purge canister valve will be closed and <br /> the sample canister valve will be opened. The initial pressure and time will be recorded. <br /> Upon reaching at least -5 in Hg or less, the sample canister valve will be closed and <br /> final pressure and time recorded. The sampling port on the sampling canister will be <br /> capped with a brass end-cap. <br /> The samples will be transported under chain-of-custody procedure to a CDPH-certified <br /> laboratory. Each sample canister will be labeled with sample designation, time, date and <br /> sampler's initials and analyzed for TPH-g, VOCs, and IPA by EPA Methods 82606 and <br /> TO-15. <br /> Advanced GeoEnviron mental,Inc. <br />