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<br /> McCampbell Analytical Inc 110 2nd Avmiie so,na #D7 1'aclieco,CA 44553-5560
<br /> Telephone 425-798-1620 Fax 925-798-1622
<br /> htCPJ/www niccanipbell coin Email beILcom
<br /> FAdvancedoEnvtronmental,Inc Chent Project ID Geweke Date Sampled 12/23/02ad Data Received 12/26/02
<br /> Stockton, CA 95215 Chem Contact Bob Marty Date Extracted 12/26/02-12/28/02
<br /> Client P 0. Date Analyzed 12/26/02-12/28/02
<br /> Volatiles Organics by P&T and GC/MS(Banc Target List)*
<br /> Ext=tMuUctho& SW5030B Ana"callatethq& SW8260B
<br /> I Werk Older 0212409
<br /> Lab ID 0212409-001 B
<br /> Client ID MW 1.
<br /> Matrix Water
<br /> Compound Concentration * DF 1 Cotnpound
<br /> Ace-toneConcetlttagon* DF 1 ND<50 10 5 0 Benzene
<br /> Bromobenzene ND<5 0ND<S 0 I0 05
<br /> 10 05 Bromoehloromethane
<br /> >3romodnchloromethane NIRS 0 10 0 S Bromoform ND<5 0 10 05
<br /> Bromomethane
<br /> 5Bromomethane ND<5 0 10 05 2-Butanone EK ND<5 0 l0 05
<br /> n-Bu benzene ND<5 0 10 0 5 sec-Bu benzene ND<10 10 10
<br /> tart-$u benzene ND<5 0 10 0 5 Carbon Ihsulfide ND<5 0 10 05
<br /> Carbon Tetrachloride ND<5 0 10 05 Chlorobenzene NIX5 0 10 0 5
<br /> Chioroethane ND<5 0 10 0 5 2-Chloroothyi Vinyl Ether NIX5 0 10 0 5
<br /> Chloroform ND<5 0 10 0 5 Chloromethane ND<5 0 10 0 5
<br /> 2-Chlorotoluene ND<5 0 10 05 4-Chlorotoluene ND<5 0 10 0 5
<br /> Drbromochlorornethane ND<5 0 10 05 1,2-Dibromo-3-chloro ro e ND<5 0 to 0 5
<br /> 1,2-Dibromoethane EDB ND<5 0 10 0 5 Dibromomethane ND<5 0 10 0 5
<br /> 1,2-Dichiorobenzene ND<5 0 10 4 5 l,3-Dichlorobenzene ND<5 0 10 0 5
<br /> 1,4-Dichlorobenzene ND<5 Q ND<5 0 10 0 S
<br /> LO 0 5 Dichlorodifluoromethane
<br /> I,1-Dichloroethane ND<5 0 10 05 1,2-Dichioroethane 1,2-DCA ND<5 0 10 05
<br /> 10 0 5 cis-I,2-Dichloroethene 5410 0 5
<br /> NIRS 0• 1,1-Dichlomethene
<br /> traits-l,2-Dichloroethene ND<5 0 10 0 5 1,2-Dichloro ane ND<5 0 10 05
<br /> 1,3-0ichloro ro ane ND<5 0 10 0 5 2,2-Dichloro ane ND<S 0 to 0 5
<br /> I,I-Dichlorora a ND<5 0 10 05 cis-1,3-Dichloro ro o ND<5 0 10 0 5
<br /> NDc5 0 10
<br /> trans-1,3-Dichlororo a ND<5 0 10 0 5 Eth lbenzene 0 5
<br /> Hexachlorobutadiene ND<5 0 10 0 5 2-Hexanone ND<5 0 10 0 5
<br /> lodomethanc <1
<br /> (Meth I iodide NDp NIRS 0 10 D 5
<br /> 10 10 4- ro t toluene ND<5 0 10 Q S
<br /> Ike ND<5 0 10 0 5 4-Meth l-2 tanone MIBK
<br /> Meth lone chloride 0 10 D 5 Meth1-t-bu 1 ether MTBE ND<5 0 !0 0 5
<br /> N hthalene ND<5 0 10 ND<5 0 1p 05
<br /> S c
<br /> O S n-Pro benzene ND<5 0 10 0 5
<br /> ND<5 0 10 0 5 l,l,I,2-Tetrachloroethane
<br /> 1,1,2 2-Tetrachlotocthane ND<5 0 10 0 5 Tetrachlorocihene ND<5 0 10 05
<br /> Toluene ND<5 0 10 0 5
<br /> 1,2,4-Trichlorobenzene ND< 0 10 0 S 1,2,3-Tnchlorobenzene ND<5 0 10 0 5
<br /> 1,12-Tnchloroethane
<br /> ND<55 0 I O O S 1,1,1-Trichloroethane ND<S 0 10 0 5
<br /> ND<5 0 10 05 Trichloroethene
<br /> Trichlorofluoromethane ND<5 0 10 0 S 1,2,3-Tnchloro ro ane ND<5 0 10 0 5
<br /> 1,2,4-Tnmeth (benzene ND<5 0 l0 0 5 1,3,5-Trrmeth Ihenzcne ND<5 0 10 0 5
<br /> Vinyl Acetate ND<50 10, 50
<br /> Vin I Chloride ND<5 0 10 D 5
<br /> X lens ND<5 0 10 0 5 ND<5 p 10 0 5
<br /> %SS 1 Surrogate Recoveries(%)
<br /> %SS3 190 %SS2 977
<br /> Comments 1
<br /> *water and vapor samples and all TCLP&SPLP extracts are reported in 99I1,soil/sludge/solid samples in
<br /> ptoduct/oilYnon-aqueous liquid samples in mg/l, N8/k& ape samples inµg/wipe,
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,i)sample diluted due to high
<br /> organic content
<br /> DHS Cezttficahon No 1644
<br /> Edward Hamilton,Lab Director
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