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EA- <br /> McCampbell Analytical Inc 110 tad Avenue South,aD7 Pacheco,CA 94553-5560 <br /> TelePhOm 925-798-1620 Fax 925-798-1622 <br /> i - 7 h J/www beiLcozn E-mail bell com <br /> FAdvanicedoEnvirommental, Inc Client Project ID Geweke <br /> Date Sampled 12/23/02 <br /> ad <br /> Date Received 12/26/02 <br /> Stockton,CA 95215 <br /> Client Contact Bob Marty Date Extracted I2/26/02-12/28/02 <br /> Client P 4 Date Analyzed 12/26/02-12/28/02 <br /> Volatiles Organics by P&T and GC/MS(Basic Target List)* _ <br /> Exttactiao Method SW5030H Analytical Method. SW9260B <br /> n <br /> Wo*Order 02I2409 Lab 1D 0212409-002B ` <br /> Client ID - MW2 <br /> Matrix _ Water <br /> Compound Concentration• DF Compound <br /> Acetone ND<20 Concentration * DF -- <br /> 1 0 5 0 Benzene <br /> Bromobenzene ND 10 05 Bromochloromethane ND 1 0 0 5 <br /> Bromodichlororn ane ND to 05 Bromoform ND l 0 0 5 <br /> Bromomethane ND 10 05 2-Butanone EK ND 1 0 0 5 <br /> n-Bu benzene ND ND 10 05 sec-Bu 1 benzene 1 0 1 0 <br /> tert-Bu benzene ND 10 05 Carbon Disulfide- ND 1 0 0 5 <br /> Carbon Tetrachloride ND 10 0 5 Cbon Dne ND ND 1 0 0 5 <br /> Chloroethane ND 10 0 5 2 ch, Vinyl Vm 1 Ether 10 0 5 <br /> Chloroform ND 1 0 0 5 Chloromethane ND 10 05 <br /> 2-Chlorotoluene ND 1 0 4 5 4-Ch]orotoluene ND to 0 5 <br /> Dtbrorriochloromethane ND 10 0 5 <br /> ND 10 05 1,2-Dibromo-3-61oro e <br /> [,2-Dibromoethane DB ND to 05 Dibrotnomethane ND 1 0 0 5 <br /> 1„2-Dichlorobenzene ND I 0 0 5 <br /> ND 1.0 05 1,3-Dichlorobenzene <br /> 1,4-Dichlorobenzestetlie ND 10 0 5 Dichlorodifluoromethane ND 1 0 0 5 <br /> l,t-Dichlotuane S <br /> ND 1 0 0 5 1,2-Dichloroethane 1,2-DCA ND 1 0 0 5 <br /> • I,i-Dichloroethene ND 10 O S cis-i,2-Dichloroethenc 1 0 O S <br /> trans-l,2-Dichloroethene ND 10 0 5 1,2-Dichlo ND a lo 0 5 <br /> 1,3-Dichla ane ND 10 0 5 2,2-Dtchlaroane ND 1 0 0 5 <br /> 1,1-Drchloro a ND ! 0 0 5 cis-1,3-Dichloro a ND 10 0 5 <br /> traits-l,3-Dichloro a ND 1 0 0 5 Eth lbenzene ND 10 0 5 <br /> Hexachlorobutadiene ND 1 0 015 2-Hexanone ND 10 0 5 <br /> lodomethane(Methyl iodide NO 10 10 4-Isro I toluene ND- 1 0 0 5 <br /> ND 10 05 <br /> Iso ro lbenzene ND <br /> ] 0 05 4Mcth 1-2- entanone IBK ND 1 0 05 <br /> Meth lene chloride ND 1 0 05 Meth I- bu I ether E <br /> N hthalene ND 1 0 0 5 n-PND 10 0 5 <br /> ro <br /> S e �n a ND 1 0 0 5 <br /> ND 10 05 1 1,1,2-Tetrachloroethane ND 1 0 0 5 <br /> 1,1,2,2-Tetrachloroethane ND 10 05 Tetrachloroethene <br /> Toluene ND 10 0 5 1,2,3-Tnchlarobenzene ND 1 0 0 5 <br /> 1,2,4-Tnchlorobenzene AID 10 o5 1,1,1-Trichloroethane ND 1 0 O S <br /> 1,1,2-Tnchloroethane ND 1 0 0 5 Trichloroethene ND 1 0 0 5 <br /> Tnchlomfluoromcthane ND 1 0 0 5 1,2,3-Troethen ane ND 10 0 5 <br /> Vinylnmeth !benzene ND 10 05 i,3,5-Tnmeth (benzene ND 1 0 0 5 <br /> Vin 1 Acetate Ali] <br /> 10 50 Vinyl Chloride ND 10 0 5 <br /> }C lens ND ] 0 0 5 ND 10 0 5 <br /> %SS l <br /> Surrogate Recoveries <br /> 107 <br /> %SS3 96 7 %SS2 991 <br /> Comments i <br /> 'water and vapor samples and all TCLP&Sp extracts <br /> extracts are reported mµg/I soiVsludgdsolid samples in <br /> product/ot1/nan-aqueous liquid samples in mg/L µlik8, wipe samples inµg/wipe, <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> h)lighter than water immiscible shem/pmduct is present,r)liquid sample that contains greater than-2 vol %sedimentd d <br /> ,1)sample diluted to high <br /> O iC ri <br /> conteL. <br /> 0 <br /> DHS Certification No 1644 <br /> t.–k—Edward Hamilton, Lab Director <br />