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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-738-1620 Fax 925-798-1622 <br /> 64http//wwwmccaml)bellcom E-mail mam@mccampbell com <br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 0203321-005 <br /> Client ID MW4/031802 <br /> Matrix W <br /> Compound Concentration* Reportrnn$Limit Compound Concentration* Reportng Limo <br /> w S w S <br /> Acetone'h ND 50 25 trans-1,3-Dichloropropene ND to 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND to 50 Ethylbenzene ND lo 50 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 50 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 10 50 <br /> Bromomethane ND 1 0 50 p-Isopropyi toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND to 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride` ND 10 5 0 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND to 50 <br /> Carbon Tetrachloride ND 10 50 Methyl tert-Butyl Ether(MTBE) ND 10 50 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 25 <br /> Chloroethane ND<5 0 1 0 50 n-Propyl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Eth ND 1 0 50 Styrene ND 10 50 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND to 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND 10 50 <br /> Dibromochloromethane ND 1 0 50 1 2,3-Tnchlorobenzene ND so 25 <br /> 1,2-13tbromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 so 1,1,1-Trichloroethane ND 10 50 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 1 0 50 1,2,3-Tnchtoropropane ND 10 50 <br /> 1,1-Dichloroethane ND 1 0 50 i,2,4-Tnmethylbenzene 1 2 10 50 <br /> 1,2-Dichloroethane 31 10 50 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate"I ND 50 25 <br /> cis-1,2-Dtchloroethene ND 1 0 50 Vinyl Chloride " ND 10 50 <br /> trans-1,2-Dtchloroethene ND 1 0 50 Xylenes,total ___92 1 05 0 <br /> 1,2-Dtchloropropane ND l 0 5 0 Comments <br /> 1,3-Dtchloropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dtchloropropane ND 1 0 50 Dibromofluoromethane 98 <br /> 1,1-Dichloropropene ND 1 0 50 Toluene-d8 93 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-Bromotluorobenzene 90 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (t)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, 0) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />