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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell co m E-mail matn@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> __[ <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab 1D 0203321-006 <br /> Client ID MWS/031802 <br /> Matrix W <br /> * Reporting Limit Repmng Limit <br /> Compound Concentration* Compound Concentration <br /> W S W S <br /> Acetone ND 50 25 trans-1,3-Dichloropropene ND 1 0 50 <br /> Benzene ND to 50 Ethylene dibromide ND 1 0 5 0 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 50 <br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25 <br /> Bromodiehloromethane ND 1 0 5 0 lodomethane ND 10 5 0 <br /> Bromoforin ND 1 0 50 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p4sopropyl toluene ND 1 0 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chloride"' ND 10 5 0 <br /> tert-Butyl benzene ND 1 0 5 0 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyi ketone ND 1 0 5 0 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl ten-Butyl Ether(MTBE) ND 1 0 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND<5 0 1 0 50 n-Propyl benzene ND 1 0 5 0 <br /> 2-Cbloroethyl Vinyl Ether(c) ND 1 0 5o Styrene ND 1 0 5 0 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 1 0 5 0 1,1,2,2-Tetrachloroethane ND 1 0 5 0 <br /> 2-Chlorotoluene ND 1 0 5 0 Tetrachloroethene ND 1 0 5 0 <br /> 4-Clilorotoluene ND 1 0 50 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 1 0 5 0 1,2,3-Tnehlorobenzene ND 5 0 25 <br /> 1,2-Dibrome-3�bloropropane ND 20 10 1,2,4-Tnehlorobenzene ND 50 25 <br /> Dibromomethane ND 1 0 50 1,1,1-Tnehloroethane ND 1 0 50 <br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 1 0 50 <br /> 1,1-Diehloroethane ND 10 50 1,2,4-Trimethyibenzene ND 10 50 <br /> 1,2-Dichlorcethane 44 1 0 50 1,3,5-Tnmethylbenzene 46 1 0 50 <br /> 1,1-Dichloroethene ND 1 0 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride ND l 0 5 0 <br /> trans-l,2-Dlchloroethene ND 1 0 50 Xylenes,total 20 1 0 5 0 <br /> 1,2-Dichloropropane ND 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND 1 0 1 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 1 Dtbromofluoromethane 102 <br /> 1,1-Dichloropropene ND l 0 5 0 Toluene-d8 71 <br /> cis-1,3-Dichioropropene ND 1 0 5 0 4-Bromofluorobenzene 86 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chlorcethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g)4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, I) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certificatron No 1644 Edward Hamilton,Lab Director <br />