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i„ <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-7918-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbell cam <br /> Advanced GeoEnvtrormental Client Protect ID Geweke Date Sampled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> Volatile Organics By GC1W <br /> EPA method 8260 <br /> Lab ID 0203321-008 <br /> Client ID MW7/031802 <br /> Matrix W <br /> Compound Concentration* Reporting Lima Compound Concentration* Reporting Limit <br /> W S W S <br /> Acetone "� ND 50 25 trans-l,3-Dichloropropene ND to 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 10 50 Sexachlorobutadiene ND 5 0 25 <br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 10 5 0 <br /> Bromoform ND 1 0 50 Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 1 0 50 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 10 S 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride° ND 10 5 0 <br /> tert-Butyl benzene ND 10 50 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketone ND 10 50 <br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) ND l 0 5 0 <br /> Chlorobenzene ND 10 50 Naphthalene ND 5 0 25 <br /> Chloroethane ND<5 0 10 5 0 n-Propyl benzene ND l 0 S 0 <br /> 2-Chloroethyl Vinyl Eth ` ND 10 5 0 Styrene ND .10 5 0 <br /> Chloroform ND 10 50 1,t,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotaiuene ND 1 0 50 Tetrachioroethene ND 1 0 5 0 <br /> 4-Chlorotoluene ND 1 0 5 0 Toluene ND 1 0 5 0 <br /> Dibromochloromethane ND 10 5 0 1,2,3-Trichlorabenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Trichlorobenzenc ND 5 0 25 <br /> Dibromomethane ND 1 0 5 0 1,1,1-Trichloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 10 50 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 5 0 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 10 5 0 <br /> IJ-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1 1-Dichloroethene ND 1 0 50 Vinyl Acetate °' ND 50 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ND 10 5 0 <br /> trans-l,2-Dichloroethene ND l 0 50 Xylenes,total ND 10 5 0 <br /> 1,2-Dichioropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 1 5 0 Dibromofluoromethane 97 <br /> 1,1-Dichloropropene ND 10 50 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 10 5 0 4-13mmofluorobenzene 88 <br /> `water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene, (d) 2-hexanone, (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol % <br /> sediment 0) sample diluted due to high organic content (k) ethenylbenzene, ( methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />