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<br /> 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560
<br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> http//www mccampbell com E-mail main@mccampbell com
<br /> Advanced GeoEnvironmental Client Project ID Geweke Date Sampled 03/18/2002
<br /> 837 Shaw Road Date Received 03/19/2002
<br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002
<br /> Client P O Date Analyzed 03/21/2002
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 0203321-009
<br /> Client ID MW8/031802
<br /> Matrix W
<br /> Compound Concentration* Reporting Unut Compound Concentration* Rep°rnng Limit
<br /> W I S W S
<br /> Acetone() ND 50 25 trans-1,3-Dichloropropene ND to 50
<br /> Benzene ND 10 50 Ethylene dibromide ND 1 0 5 0
<br /> Bromobenzene ND 10 5 0 Ethylbenzene ND 1 0 50
<br /> Bromochloromethane ND 1 0 5 0 Hexachlorobutadiene ND 5 0 25
<br /> Bromodichloromethane ND 1 0 50 Iodomethane ND 1 0 5 0
<br /> Bromoform ND 1 0 5 0 Isopropylbenzene ND 1 0 50
<br /> Bromomethane ND 10 5 0 p4sopropyl toluene ND 1 0 5 0
<br /> n-Butyl benzene ND l 0 5 0 Methyl butyl ketone ND 1 0 5 0
<br /> sec-Butyl benzene ND 1 0 5 0 Methylene Chloride"' ND 1 0 5 0
<br /> tert-Butyl benzene ND 1 0 5 0 Methyt ethyl ketone ND 2 0 10
<br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone a ND 10 50
<br /> Carbon Tetrachloride ND 1 0 5 0 Methyl tert-Butyl Ether(MTBE) ND 1 0 5 0
<br /> Chlorobenzene ND 1 0 5 0 Naphthalene 12 5 0 25
<br /> Chloroethane ND<S 0 1 0 50 n-Propyl benzene ND 1 0 5 0
<br /> 2-Cbloroethyl Vinyl Ether" ND 10 5 0 Styrene ND 1 0 5 0
<br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 1 0 5 0
<br /> Chlaromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50
<br /> 2-Chlorotoluene ND 10 5 0 Tetrachloroethane ND 1 0 5 0
<br /> 4-Chlorotoluene ND 1 0 5 0 Toluene 11 ND 10 5 0
<br /> Dibrumochloromethane ND 1 0 5 0 1,2,3-Tnchlorobenzene ND 50 25
<br /> 1,2-Dibromo-3-chloropropane ND 2 0 10 1,2,4-Tnchlorobenzene ND 50 25
<br /> Dibromomethane ND 1 0 5 0 1,1,1-Trichloroethane ND 1 0 5 0
<br /> 1,2-Dichlorobenzene ND 1 0 5 0 1,1,2-Tnchloroethane ND 1 0 5 0
<br /> 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 5 0
<br /> 1,4-Dichlorobenzene ND 1 0 50 Tnchlorotluoromethane ND 1 0 5 0
<br /> Dichlorodifluoromethane ND 1 0 5 0 1,2,3-Tnchloropropane ND 10 5 0
<br /> I,1-Dichtoroethane ND 1 0 5 0 1,2,4-Tnmethylbenzene 15 1 0 5 0
<br /> 1,2-Dichloroethane 2 4 1 0 50 1,3,5-Tnmethylbenzene 2 4 10 5 0
<br /> I,i-Dichloroethene ND 1 0 5 0 Vinyl Acetate m ND 50 25
<br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride " ND 1 0 5 0
<br /> trans-l,2-Dichloroethene ND 10 50 Xylenes,total 5 8 1 0 5 0
<br /> 1,2-Dichloropropane ND 10 50 Comments
<br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND 10 50 Dibromofluoromethane 97
<br /> 1,1-Dtchloropropene ND L10 1 50 Toluene-d8 96
<br /> cis-1,3-Dtchloropropene ND [1_6 5 0 4-Bromofluorobenzene 88
<br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysts
<br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (0 2-butanone, (g) 4-methyl-2-
<br /> • pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (t)liquad sample that contains greater than--5 vol %
<br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, ( methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hanulton, Lab Director
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