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I 10 2nd Avenue South,#137,Pacheco,CA 94553-5560 y <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br /> Advanced Geolanvirorunental Client Protect ID Geweke <br /> Date Sainpled 03/18/2002 <br /> 837 Shaw Road Date Received 03/19/2002 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002 <br /> Client P O Date Analyzed 03/21/2002 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 0203321-014 <br /> Client 1D MW 1 3/03 1 802 <br /> Matrix W <br /> Compound Concentration* RepomngLumt Compound Concentration* RepcmngUmit <br /> W I S W I S <br /> Acetone ND 50 25 trans-l,3-Dichloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 50 <br /> Bromobenzene ND 1 0 50 Ethylbenzene ND 1 0 50 <br /> Bromochlommethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 50 lodomethane ND 10 50 <br /> Bromoforrn ND 1 0 50 Isopropylbenzene ND 1 0 50 <br /> Bromomethane ND 1 0 50 p4sopropyl toluene ND 1 0 5 0 <br /> n-Butyl benzene ND 10 50 Methyl butyl ketone ND 1 0 5 0 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND 1 0 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 1 0 50 Methyl isobutyl ketone ND 1 0 50 <br /> . Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(MTBE) ND 10 50 <br /> Chlorobenzene ND 1 0 50 Naphthalene ND 50 25 <br /> Chloroethane ND<5 0 1 0 50 n-Propyl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Etherle' ND 1 0 50 Styrene M ND to 50 <br /> Chloroform ND 1 0 50 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 1 0 50 1,1,2,2-Tetrachloroethane ND 1 0 50 <br /> 2-Chlorotoluene ND 1 0 50 Tetrachloroethene ND 10 50 <br /> 4-Chlorotoluene ND 1 0 50 Toluene ND to so <br /> Dibromochloromethane ND 10 50 1,2,3-Trichlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 50 1,1,1-Tnchloroethane ND 1 0 5 0 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 1 0 50 <br /> 1,3-Dichlorobenzene ND 10 50 Trichloroethene ND 10 50 <br /> 1,4-Dichlorobenzene ND 10 50 Trichlorofluoromethane ND 10 50 <br /> Dichlorodifluoromethane ND 10 50 1,2,3-Tnchloropropane ND to 50 <br /> 1,1-Dichloroethane ND 10 50 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 50 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 50 Vinyl Acetate 01 ND 50 25 <br /> cis-1,2-Dichloroethene ND 10 50 Vinyl Chloride kM ND to 50 <br /> trans-1,2-Dichloroethene ND 1 0 50 Xylenes,total ND 1 0 50 <br /> 1,2-Dichloropropane ND 1 0 50 Comments <br /> 1,3-Dichloropropane ND 1 0 50 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 50 Dibromofluoromethane 97 <br /> 1,1-Dichloropropenc ND t 0 50 Toluene-d8 95 <br /> cis-1,3-Dichloropropene ND 1 0 50 4-BTomofluorobenzene 87 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d)2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, ) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />