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<br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560
<br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> h //www mccam bell coin E-mail main@mccampbell corn
<br /> Advanced GeoEnviromnental Client Project ID Geweke Date Sampled 03/18/2002
<br /> 837 Shaw Road Date Received 03/19/2002
<br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 03/21/2002
<br /> [Client P O Date Analyzed 03/21/2002
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab 1D 0203321-015
<br /> Client 1D MW 1 4/03 1 802
<br /> Matrix W
<br /> Compound Concentration* Reporting U t Compound Concentration* Reporting Lunt
<br /> W S —77 S
<br /> Acetone to ND<500 50 25 trans-1,3-Dichloropropene ND<50 10 50
<br /> Benzene 1200 1 0 5 0 Ethylene dibromide ND<50 1 0 5 0
<br /> Bromobenzene ND<50 10 5 0 Ethylbenzene 100 10 50
<br /> Bromochloromethane ND<50 1 0 5 0 Hcxachlorobutadiene ND<50 5 0 25
<br /> Bromodichloromethane ND<50 10 50 Iodomethane NDa50 10 5 0
<br /> Bromoform ND<50 1 0 50 Isopropylbenzene ND<50 to 5 0
<br /> Bromomethane ND<50 1 0 5 0 p-Isopropyl toluene ND<50 10 50
<br /> n-Butyl benzene ND<50 1 0 5 0 Methyl butyl ketone ND<50 10 50
<br /> sec-Butyl benzene ND<50 1 0 50 Methylene Chlonde` ND<70 10 50
<br /> tert-Butyl benzene ND<50 1 0 50 Methyl ethyl ketone ND<100 2 0 10
<br /> Carbon Disulfide ND<50 1 0 5 0 Methyl isobutyl ketone ND<50 to 5 0
<br /> Carbon Tetrachloride ND<50 1 0 5 0 Methyl tent-Butyl Ether(MTBE) ND<50 10 50
<br /> Chlorobenzene ND<50 1 0 5 0 Naphthalene ND<50 50 25
<br /> Chloroethane ND<150 10 5 0 n-Propyl benzene ND<50 10 5 0
<br /> 2-Chloroethyl Vinyl Ethe ` NIX100 to 5 0 Styrene M ND<50 to 50
<br /> Chloroform ND<50 10 5 0 1,1,1,2-Tetrachloroethane ND<50 10 50
<br /> Chloromethane ND<50 10 5 0 1,1,2,2-Tetrachloroethane ND<50 10 50
<br /> 2-Chlorotoluene ND<50 10 50 Tetrachloroethene NI]<50 10 50
<br /> 4-Chlorotoluene ND<50 10 50 Toluene W 78 10 50
<br /> Dibromochloromethane ND<50 10 50 1,2,3-Tnchlorobenzene ND<50 5 0 25
<br /> 1,2-Dibrome-3-chloropropane ND<50 20 10 1,2,4-Tnchlorobenzene ND<50 5 0 25
<br /> Dibromomethane ND<50 1 0 5 0 1,1,1-Tnchloroethane NLX50 1 0 50
<br /> 1,2-Dichlorobenzene ND<50 10 5 0 1,1,2-Tnchloroethane ND<50 10 5 0
<br /> 1,3-Dichlorobenzene ND<50 1 0 5 0 Trichloroethene ND<50 1 0 50
<br /> 1,4-Dichlorobenzene ND<50 10 50 Tnchlorofluoromethane ND<50 10 50
<br /> Dichlorodifluoromethane ND<50 10 50 1,2,3-Trtchloropropane ND<50 1 0 50
<br /> 1,1-Dichloroethane ND<50 to 5 0 1,2,4-Tnmethylbenzene 72 10 50
<br /> 1,2-Dichloroethane ND<50 to 5 0 1,3,5-Tnmethylbenzene ND<50 1 0 50
<br /> 1,1-Dichloroethene ND<50 1 0 50 Vinyl Acetate ND<500 50 25
<br /> cis-1,2-Dichloroethene ND<50 1 0 5 0 Vinyl Chloride ° N13<50 1 0 50
<br /> trans-l,2-Dichloroethene ND<50 1 0 5 0 Xylenes,total 350 1 0 5 0
<br /> 1,2-Dichlaropropane ND<50 10 50 Comments
<br /> 1,3-Dichloropropane ND<50 1 0 50 Surrogate Recoveries(%)
<br /> 2,2-Dichloropropane ND<50 10 50 Dibromofluoromethane 89
<br /> 1,1-Dichloropropene ND<50 1 0 50 1 Toluene-d8 93
<br /> cis-1,3-Dichloropropene ND<50 10 50 4-Bromofluorobenzene 86
<br /> water and vapor samples are reported to ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d)2-hexanone, (e) dichloromethane, (f)2-butanone, (g)4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %
<br /> is sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n)
<br /> chloroethene,(o)dimethylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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