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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAN PBELL ANALYTICAL INC. , Telephone:925-798-1620 Fax : 925-798-1622 - <br /> 44 http://www.mccampbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/15/00 <br /> 4005 North Wilson Way Date Received: 12/20/00 <br /> IStockton,CA 95205 Client Contact: Brian Millman Date Extracted: 12/22-12/26/00 <br /> Client P.O: Date Analyzed: 12/22-12/26100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 56438 <br /> Client ID MW7/121500 <br /> Matrix W <br /> Compound Concentration* Repotting Limit Compound Concentration* Reporting Limit <br />' W S W S <br /> Acetone(b) ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND 1.0 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br /> I Bromochloromethane ND 1.0 5.0 E-lexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND LO 5.0 lodomethane ND 1.0 5.0 <br /> Bromoform ND 1.0 5.0 Isopropylbenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyi butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride"' ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br />'. Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketone Cgr ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.0 5.0 Methyl tert-Butyi Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br />' 2-Chloroethyl Vinyl Ether'!:) ND 1.0 5.0 Styrene NA 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5A <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoluene ND 1.0 5.0 Tetrachloroethene ND<2.0 1.0 5.0 <br />' 4-Chlorotoluene ND 1.0 5.0 Toluene ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND 2.0 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br />' 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloraethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br />' <br /> 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichioroethane 1.7 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 L5O <br /> I,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 <br /> cis-1,2-Di chloroethene ND 1.0 5.0 Vinyl Chloride " ND 1.0 <br />' trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND lA <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 109 <br />' 1,1-Dichloropropene ND 1.0 5.0 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND 1.0 5.0 4-Bromofluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c)(2-chloroethoxy) ethene; (d) 2-hexanone; (e)dichloromethane; (f) 2-butanone; (g)4-methyl-2- <br /> • pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than--5 vol. °/O <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> t <br />