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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. TelephoneT925-798-1620 925-798-1620 Fax: 925-798-1622 <br /> Ihttpa/www.mcc4Tpbell.com E-mail: main@mccampbell.com <br /> • <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/15/00 <br /> 4005 North Wilson Way 'Date Received: 12/20/00 <br /> Stockton, CA 95205 Client Contact:Brian Millman Date Extracted: 12/22-12/26/00 <br /> I Client P.O: Date Analyzed: 12122-12/26/00 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 56439 <br /> Client ID MW81121500 <br /> Matrix W <br /> Reporting Limit Reywning Limit <br /> Compound Concentration* Compound Concentration* <br />' W S W S <br /> Acetone(b) ND<20 5.0 25 trans-l,3-Dichloropropene ND<5.0 1.0 5.0 <br /> Benzene ND<5.0 1.0 5.0 Ethylene dibromide ND<5.0 1.0 5.0 <br /> Bromobenzene ND<5.0 1.0 5.0 Ethylbenzene 1 98., 1.0 5.0 <br />' Bromochloromethane ND<5.0 1.0 5.0 Hexachlorobutadiene ND<5.0 5.0 25 <br /> Bromodichloromethane ND<5,0 1.0 5.0 lodomethane ND<5,0 1.0 5.0 <br /> Bromoform ND<5.0 1.0 5.0 Isopropylbenzene 29 1.0 5.0 <br /> Bromomethane ND<5.0 1.0 5.0 p-Isopropyl toluene ND<5.0 1.0 5.0 <br />' n-Butyl benzene ND<5.0 1.0 5.0 Methyl butyl ketone ND<5.0 1.0 5.0 <br /> sec-Butyl benzene ND<5.0 1.0 5.0 Methylene Chloride(e) ND<15 1.0 5.0 <br /> tert-Butyl benzene ND<5.0 1.0 5.0 Methyl ethyl ketone ND<5.0 2.0 10 <br />' Carbon Disulfide ND<5.0 1.0 5.0 Methyl isobutyl ketone ND<5.0 1.0 5.0 <br /> Carbon Tetrachloride ND<5.0 1.0 5.0 Methyl tcrt-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlorobenzene ND<5.0 1.0 5.0 Naphthalene ND<5.0 5.0 5.0 <br /> Chloroethane ND<5.0 1.0 5.0 n-Propyl benzene 46 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ether` ND<5.0 1.0 5.0 Styrene ND<5.0 1.0 5.0 <br />' Chloroform ND<5.0 1.0 5.0 1,3,1,2-Tetrachloroethane ND<5.0 1.0 5.0 <br /> Chloromethane ND<5.0 1.0 5.0 1,1,2,2-Tetrachloroethane ND<5.0 1.0 5.0 <br /> 2-Chlorotoluene ND<5.0 1.0 5.0 Tetrachloroethene ND<5.0 1.0 5.0 <br />' 4-Chlorotoluene ND<5.0 1.0 5.0 Toluene"'— ND<5.0 1.0 5.0 <br /> Dibromochloromethane ND<5.0 1.0 5.0 1,2,3-Trichlorobenzene ND<5.0 5.0 25 <br /> 1,2-Dibromo-3-chloropropane ND<5.0 2.0 10 1,2,4-Trichlorobenzene ND<5.0 5.0 25 <br /> Dibromomethane ND<5.0 1.0 5.0 1,1,1-Trichloroethane ND<5.0 1.0 5.0 <br />' 1,2-Dichlorobenzene ND<5.0 1.0 5.0 1,1,2-Trichloroethane ND<5.0 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<5.0 1.0 5.0 Trichloroethene ND<5.0 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<5.0 1.0 5.0 Trichlorofluoromethane ND<5.0 1.0 5.0 <br /> Dichlorodifluoromethane NLK5.0 1.0 5.0 1,2,3-Trichloropropane ND<5.0 1.0 5.0 <br /> 1,1-Dichloroethane ND<5.0 1.0 5.0 1,2,4-Trimethylbenzene 250 1.0 5.0 <br />' 1,2-Dichloroethane 15 1.0 5.0 1,3,5-Trimethylbenzene 53 1.0 5.0 <br /> l,l-Dichloroethene ND<5.0 K1.0 <br /> 5.0 Vinyl Acetate '" ND<5.0 5.0 25 <br /> cis-1,2-Dichloroethene ND<5.0 5.0 Vinyl Chloride ° ND<5.0 1.0 5.0 <br />' trans-1,2-Dichloroethene ND<5.0 5.0 Xylenes,total 150 1.0 5.0 <br /> 1,2-Dichloropropane ND<5.0 5.0 Comments: <br /> 1,3-Dichloropropane ND<5.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<5.0 5.0 Dibromofluoromethane 106 <br /> I,I-Dichloropropene ND<5.0 5.0 Toluene-d8 99 <br /> cis-1,3-Dichloropropene ND<5.0 1.0 5.0 4-Bromotluorobenzene 101 <br /> water and vapor samples are reported in ug(L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy)cthene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol.% <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; 1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> 1 <br />