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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone- 925-798-1620 Fax : 925-798-1622 <br />' 14 http://www.mccampbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/15/00 <br /> 4005 North Wilson Way Date Received: 12/20/00 <br />' Stockton, CA 95205 Client Contact: Brian Millman Date Extracted: 12/22-12/26/00 <br />' Client P.O: Date Analyzed: 12/22-12/26/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 56441 <br />' Client ID MW11/121500 <br /> Matrix W <br /> Rcpocting Limit * Reporting Limit <br /> Compound Concentration Compound Concentration <br />' W S W S <br /> Acetone ND 5.0 25 trans-1,3-Dichloropropene ND 1.0 5.0 <br /> Benzene ND 1.0 5.0 Ethylene dibromide ND Lo 5.0 <br /> Bromobenzene ND 1.0 5.0 Ethylbenzene ND 1.0 5.0 <br />' Bromochloromethane ND 1.0 5.0 Hexachlorobutadiene ND 5.0 25 <br /> Bromodichloromethane ND 1.0 5.0 Iodomethane ND 1.0 5.0 <br /> Bromoform ND Lo 5.0 lsopropyibenzene ND 1.0 5.0 <br /> Bromomethane ND 1.0 5.0 p-Isopropyl toluene ND 1.0 5.0 <br />' n-Butyl benzene ND 1.0 5.0 Methyl butyl ketone ND 1.0 5.0 <br /> sec-Butyl benzene ND 1.0 5.0 Methylene Chloride7'7- ND 1.0 5.0 <br /> tert-Butyl benzene ND 1.0 5.0 Methyl ethyl ketone ND 2.0 10 <br /> Carbon Disulfide ND 1.0 5.0 Methyl isobutyl ketones ND 1.0 5.0 <br /> Carbon Tetrachloride ND 1.o 5.0 Methyl tert-Butyl Ether(MTBE) --- 1.0 5.0 <br /> Chlorobenzene ND 1.0 5.0 Naphthalene ND 5.0 5.0 <br /> Chloroethane ND 1.0 5.0 n-Propyl benzene ND 1.0 5.0 <br />' 2-Chloroethyl Vinyl Ethe ND, 1.0 5.0 Styrene ND 1.0 5.0 <br /> Chloroform ND 1.0 5.0 1,1,1,2-Tetrachloroethane ND 1.0 5.0 <br /> Chloromethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 <br /> 2-Chlorotoiuene ND 1.0 5.0 Tetrachloroethene ND<2.0 1.0 5.0 <br />' 4-Chlorotoluene ND 1.0 5.0 Toluene 01ND 1.0 5.0 <br /> Dibromochloromethane ND 1.0 5.0 1,2,3-Trichlorobenzene ND 5.0 25 <br /> 1,2-Dibromo-3-chlorepropane ND 2.0' 10 1,2,4-Trichlorobenzene ND 5.0 25 <br /> Dibromomethane ND 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 <br />' 1,2-Dichlorobenzene ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 <br /> 1,3-Dichlorobenzene ND 1.0 5.0 Trichloroethene ND 1.0 5.0 <br /> 1,4-Dichlorobenzene ND 1.0' 5.0 Trichlorofluoromethane ND 1.0 5.0 <br /> Dichlorodifluoromethane ND 1.0 5.0 1,2,3-Trichloropropane ND 1.0 5.0 <br />' 1,1-Dichloroethane ND 1.0 5.0 1,2,4-Trimethylbenzene ND 1.0 5.0 <br /> 1,2-Dichloroethanc ND 1.0 5.0 1,3,5-Trimethylbenzene ND 1.0 5.0 <br /> 1,1-Dichloroethene ND 1.0 5.0 Vinyl Acetate m ND 5.0 25 <br /> cis-1,2-Dichloroethene ND 1.0 5.0 Vinyi Chloride ° ND 1.0 5.0 <br />' trans-1,2-Dichloroethene ND 1.0 5.0 Xylenes,total ND 1.0 1 5.0 <br /> 1,2-Dichloropropane ND 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1.0 5.0 Dibromofluoromethane 106 <br /> t 1,1-Dichloropropene ND 1.0 5.0 Toluene-dg 97 <br /> cis-1,3-Dichloropropene ND ].0 5.0 4-Bromotluorobenzene 107 <br /> 'water and vapor samples are reported in ug/i.,soil and sludge samples in ug/kg,wipes in ug/wipe and'all TCLP/SPLP extracts in ug/L <br /> t ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; 1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />