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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone-925-798-1620 Fax: 925-798-1622 <br /> ihttp://www.mccaml)bcll.com E-mail:main@mccampbell.com <br /> i• <br /> iAdvanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/15/00 <br /> 4005 North Wilson Way Date Received: 12/20/00 <br /> Stockton, CA 95205 Client Contact:Brian Millman Date Extracted: 12/22-12126/00 <br /> CIient P.O: Date Analyzed: 12122-12/26100 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 56440 <br />' Client ID NIW9/121500 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Reporting Limit <br /> Compound Concentration* <br /> W S W S <br /> Acetone ND<5.0 5.0 25 trans-1,3-Dichloropropene ND<2.5 1.0 5.0 <br /> Benzene ND<2.5 1.0 5.0 Ethylene dibromide ND<2.5 1.0 5.0 <br /> Bromobenzene ND<2.5 1.0 5.0 Ethylbenzene 53 1.0 5.0 <br />' Bromochloromethane ND<2.5 1.0 5.0 Hexachlorobutadiene ND<5.0 5.0 25 <br /> Bromodichloromethane ND<2.5 1.0 5.0 lodomethane ND<2.5 1.0 5.0 <br /> Bromoform ND<2.5 1.0 5.0 Isopropylbenzene 17 1.0 5.0 <br /> Bromomethane ND<2.5 1.0 5.0 p-Isopropyl toluene ND<2.5 1.0 5.0 <br />' n-Butyl benzene ND<2.5 1.0 5.0 Methyl butyl ketone ND<2.5 1.0 5.0 <br /> sec-Butyl benzene ND<2.5 1.0 5.0 Methylene Chloride") ND<10 1.0 5.0 <br /> tert-Butyl benzene ND<2.5 1.0 5.0 Methyl ethyl ketone ND<2.5 2.0 l0 <br /> Carbon Disulfide ND<2.5 1.0 5.0 Methyl isobutyi ketone ND<2.5 1.0 5.0 <br />' Carbon Tetrachloride ND<2.5 1.0 5.0 Methyl tert-Butyl Ether(MTBE) 1.0 5.0 <br /> Chlombenzene ND<2.5 1.0 5.0 Naphthalene ND<5.0 5.0 5.0 <br /> Chloroethane ND<2.5 1.0 5.0 n-Propyl benzene 32 1.0 5.0 <br /> 2-Chloroethyl Vinyl Ethe ND<2.5 1.0 5.0 Styrene NLX2.5 1.0 5.0 <br />' Chloroform ND<2.5 1.0 5.0 1,1,1,2-Tetrachloroethane ND<2.5 1.0 5.0 <br /> Chloromethane ND<2.5 1.0 5.0 1,1,2,2-Tetrachloroethane ND<2.5 1.0 5.0 <br /> 2-Chlorotoluene ND<2.5 1.0 5.0 Tetrachloroethene ND<2.5 1.0 5.0 <br />' 4-Chlorotoluene ND<2.5 LO 5.0 Toluene ND<2.5 1.0 5.0 <br /> Dibromochloromethane ND<2.5 1.0 5.0 1,2,3-Trichlorobenzene ND<5.0 5.0 25 <br /> 1,2-Dibromo-3-chlorapropane ND<2.5 2.0 10 1,2,4-Trichlorobenzene ND<5.0 5.0 25 <br /> Dibromomethane ND<2.5 1.0 5.0 1,1,1-Trichloroethane ND<2.5 1.0 5.0 <br />' 1,2-Dichlorobenzene ND<2.5 1.0 5.0 1,1,2-Trichloroethane ND<2.5 1.0 5.0 <br /> 1,3-Dichlorobenzene ND<2.5 1.0 5.0 Trichloroethene ND<2.5 1.0 5.0 <br /> 1,4-Dichlorobenzene ND<2.5 1.0 5.0 Trichlorofluoromethane ND<2.5 1.0 5.0 <br /> Dichlorodifluoromethane ND<2.5 1.0 5.0 1,2,3-Triehloropropane ND<2.5 1.0 5.0 <br /> l,l-Dichloroethane ND<2.5 1.0 5.0 1,2,4-Trimethylbenzene 96 1.0 5.0 <br />' . 1,2-Dichloroethane 36 1.0 5.0 1,3,5-Trimethylbenzene 26 1.0 5.0 <br /> 1,1-Dichloroethene ND<2.5 1.0 5.0 Vinyl Acetate"I ND<5.0 5.0 25 <br /> cis-1,2-Dichloroethene ND<2.5 1.0 5.0 Vinyl Chloride " ND<2.5 1.0 5.0 <br />' trans-1,2-Dichloroethene ND<2.5 1.0 5.0 Xylenes,total 17 1.0 5.0 <br /> 1,2-Dichloropropane ND<2.5 1.0 5.0 Comments: <br /> 1,3-Dichloropropane ND<2.5 1.0 5.0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<2.5 1.0 5.0 Dibromofluoromethane 104 <br /> 1,1-Dichloropropene ND<2.5 1.0 5.0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND<2.5 1.0 5.0 4-Bromofluorobenzene 99 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L. <br />' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d)2-hexanone; (e) dichloromethane; (f)2-butanone; (g)4-methyl-2- <br /> �� pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than--5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; ( methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> t chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />