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110 Second Avenue South,#D7,Pacheco,CA 94553-5560_ <br /> F44 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> hap://www.rnccampbel1.co E-mail:main@mccarnpbell.com <br /> Advanced GeoEnvironmental CIient Project TD:Geweke Date Sampled: 03/17/99 <br />' 4005 North Wilson Way Date Received: 03/19/99 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 03/21-03124199 <br /> Client P.O: Date Analyzed: 03/21-03/24/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8264 <br /> Lab 1D 05359 <br /> Client 1D MW-1 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<3 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> Brornochloromethane ND Isopropylbenzene ND <br />' Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> set-Butyl benzene ND Methyl isobutyl ketone'R ND <br /> tert-Butyl benzene ND Methyl teri-Butyl Ether(MTBE) <br /> Carbon Disulfide 1.9 Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Ile Chlorobenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether"I ND 1,1,2,2-Tetrachioroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene ND <br /> 2-010r010luene ND 1,2,3-Trichl orobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochlommethane ND 1,1,1-Trichloroethane ND <br />' 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br />' 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethyibenzene ND <br /> LI-Dichloroethane ND Vinyl Acetate"" - 1.7 <br /> 1,2-Dichloroethane 1.3 Vinyl Chloride'") ND <br />' 1,1-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br />' 1,2-Dichloroprop2ne ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br />' cis-1,3-Dichloropropene ND Dibromofluoromethane 93 <br /> trans-1,3-Dichloropropene ND Toluene-d8 101. <br /> Ethylene dibromide ND 4-Bromofluorobenzene 108 <br /> 'water and vapor samples are reported in ug1,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment;0)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n}chloroethene;(o}dimethylbenzenes. <br /> DHS Certification No. 1644 // Edward Hamilton, Lab Director <br />