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I 110 Second Avenue South,##137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htW://www.mccamnbeli.com E-mail:main@mccampbell.com <br /> I <br /> Advanced GeoEnvironmental Client Project ID:Geweke Date Sampled: 03/17/99 <br /> 4005 North Wilson Way <br /> Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact:Kevin McKibben Date Extracted: 03121-03124199 <br /> [Client P.O: Date Analyzed: 03/21-03/24/99 <br /> Volatile Organics By GC/MS <br />' EPA method 8260 <br /> Lab ID 05360 <br /> Client ID MW-2 <br /> I Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<3 Ethylbenzene ND <br /> I Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chloride` ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone ND <br /> ten-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene` ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroeth2ne ND <br /> 2-Chloroethyl Vinyl Ether ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethane ND <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1.2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene ND <br /> I,l-Dichloroethane ND Vinyl Acetate" 2.6 <br /> 1,2-Dichloroethane ND Vinyl Chloride " ND <br /> l,l-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 88 <br /> I <br /> trans-l,3-Dichloropropene ND Toluene-0 113 <br /> Ethylene dibromide ND 4-Bromofluarobenzene 92 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ugAg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> I Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2u&/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> I sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyse;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 /,/ Edward Hamilton,Lab Director <br /> I <br />