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110 Second Avenue South,#t'D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax-. 925-798-1622 <br /> / E-mail:main@amcewnpbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/17/99 <br /> I4005 North Wilson Way Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 03/21-03/24/99 <br /> Eent .O: Date Analyzed: 03/21-03/24/99 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 05361 <br /> Client ID MW-3 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2.5 Ethylbenzene ND<2.5 <br />' Benzene ND<2.5 Hexachiorobutadiene ND<2.5 <br /> Bromobenzene NDX2.5 Iodomethane ND<2.5 <br /> Bromochloromethane ND<2.5 Isopropylbenzene ND<2.5 <br /> Bromodichloromethane ND<2.5 p-Isopropyl toluene ND<2.5 <br />' Bromoform ND<2.5 Methyl butyl ketoneND<2.5 <br /> Bromomethane ND<2.5 Metbylene Chloride" ND<2.5 <br /> n-Butyl benzene ND<2.5 Methyl ethyl ketone ND<2.5 <br />' sec-Butyl benzene ND<2.5 Methyl isobutyl ketones ND<2.5 <br /> tert-Butyl benzene ND<2.5 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<2.5 Napthalene ND<2.5 <br /> Carbon Tetrachloride ND<2.5 n-Propyl benzene ND<2.5 <br />' Chlorobenzene ND<2.5 Styrene ND<2.5 <br /> Chloroethane NDc2.5 1,1,1,2-Tetrachloroethane ND<2.5 <br /> 2-Chloroethyl Vinyl Ether ND<2.5 1,1,2,2-Tetrachloroethane ND<2.5 <br /> Chloroform ND<2.5 Tetrachloroethene ND<2.5 <br /> I Chloromethane ND<2.5 Toluene NIK2.5 <br /> 2-Chlorotoluene ND<2.5 1,2,3-Trichlorobenzene ND<2.5 <br /> 4-Chlorotoluene ND<2.5 1,2,4-Trichl orobenzene ND<2.5 <br /> Dibromochloromethane ND<2.5 1,1,1-Trichloroethane ND<2.5 <br /> 1,2-Dibromo-3-chloropropane ND<2.5 1,1,2-Trichloroethane ND<2.5 <br /> Dibromomethane ND<2.5 Trichloroethene ND<2.5 <br /> 1,2-Dichlorobenzene ND<2.5 Trichlorofluoromethane ND<2.5 <br /> 1,3-Dichlorobenzene ND<2.5 1,2,3-Trichloropropane ND<2.5 <br />' 1,4-Dichlorobenzene 2.9 1,2,4-Trimethyibenzene ND<2.5 <br /> Dichlorodifluoromethane ND<2.5 1,3,5-Trimethylbenzene ND<2.5 <br /> 1,1-Dichloroethane ND<2.5 Vinyl Acetate 1' ND<2.5 <br /> 1,2-Dichloroethane 60 Vinyl Chloride " ND<2.5 <br />' 1,1-Dichloroethene ND<2.5 Xylenes,total `° ND<2.5 <br /> cis-1,2-Dichloroethene ND<2.5 <br /> trans-l,2-Dichloroethene ND<2.5 <br /> 1,2-Dichloropropane ND<2.5 <br /> 1,3-Dichloropropane ND<2.5 <br /> 2,2-Dichloropropane ND<2.5 Comments: <br /> I,1-Dichloropropene ND<2.5 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<2.5 Dibromofluoromethane 93 <br /> I <br /> trans-l,3-Dichloropropene ND<2.5 Toluene-d8 109 <br /> Ethylene dibromide ND<2.5 4-Bromofluorobenzene 107 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hex2none; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylaeetone;(h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than -5 vol. % <br /> sediment;0)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1544 // Edward Hamilton, Lab Director <br /> I <br />