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110 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hnp•/ E-mail: main@tnccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/17/99 <br /> I4005 North Wilson Way Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact:Kevin McKibben Date Extracted: 03/21-03/24/99 <br /> IClient P.O: Date Analyzed: 03/21-03/24/99 <br /> I Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 05371 <br /> Client ID MW-13 <br /> I Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<3 Ethylbenzene 4.6 <br /> I Benzene ND Hexachlorobutadiene NO <br /> Bromobenzene NO lodomethane NO <br /> Bromochloromethane ND lsopropylbenzene NO <br /> Bromodichloromethane ND p-lsopropyl toluene NO <br /> I Bromoform ND Methyl butyl ketone NO <br /> Bromomethane ND Metbylene Chloride") NO <br /> n-Butyl benzene NO Methyi ethyl ketone NO <br /> sec-Butyl benzene ND Metbyl isobutyl ketoneNO <br /> tert-Butyl benzene NO Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide NO Napthalene NO <br /> Carbon Tetrachloride NO n-Propyl benzene NO <br /> Chlorobenzene NO Styrene NO <br /> Chloroethane ND 1,1,1,2-Tetr2chloroethane ND <br /> 2-Chioroethyl Vinyl Ether") NO 1,1,2,2-Tetrachloroeth2ne NO <br /> Chloroform NO Tetrachloroethene NO <br /> Chloromethane ND Toluene 9.4 <br /> 2-Chlorotoiuene NO 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichiorobenzene ND <br /> Dibromochloromethane NO 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane NO 1,1,2-Trichloroethane NO <br /> Dibromomethane NO Trichloroethene NO <br /> 1,2-Dichlorobenzene NO Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene NO 1,2,4-Trimethylbenzene 7.3 <br /> Dichlorodifluoromethane NO 1,3,5-Trimethylbenzene 1.9 <br /> ],1-Dichloroethane ND Vinyl Acetate"" NO <br /> 1,2-Dichloroethane ND Vinyl Chloride'"O NO <br /> 1,1-Dicbloroethene ND Xyl enes,totai 22 <br /> cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene NO <br /> 1,2-Dichloropropane NO <br /> I 1,3-Dichloropropane NO <br /> 2,2-Dichloropropane NO Comments: <br /> 10-Dichloropropene NO Surrogate Recoveries{%) <br /> cis-1,3-Dichloropropene NO Dibromofluoromethane 94 <br /> trans-l,3-Dichloropropene NO Toluene-dg 121. <br /> Ethylene dibromideLJ NO 4-Bromofluorobenzene 104 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe NO means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chioroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 i Edward Hamilton,Lab Director <br /> I <br />