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' 110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCA.MPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br /> hJW:/Jwww.mccampbcll.co E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/17/99 <br />' 4005 North Wilson Way Date Received: 03/19/99 <br />' Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 03/21-03124199 <br /> Client P.O: Date Analyzed: 03/21-03/24/99 <br />' Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 05372 <br /> Client ID MW-14 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<3 Ethylbenzene 1.9 <br />' Benzene 1.9 Hexachlorobutadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br />' Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketoneND <br /> Bromomethane ND Methylene Chloridel`) ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br />' sec-Butyl benzene ND Methyl isobutyl ketone`g ND <br /> tent-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether�'3 ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroetbenc ND <br />' Chloromethane ND Toluene 7.2 <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobcnzenc ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br />' 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene 7.5 <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene 3.8 <br /> 1,1-Dichloroethane ND Vinyl Acetate" ND <br /> 1,2-Dichloroethane 4.7 Vinyl Chloride " ND <br />' <br /> 7,l-Dichloroethane ND Xylenes,total 43 <br /> cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br />' 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> I cis-1,3-Dichloropropene ND Dibromofluoromethanc 92 <br /> trans-1,3-Dichloropropene ND Toluene-d8 110. <br /> Ethylene dibromide ND 4-BTomofluorobenzene 102 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2uglwipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 /,' Edward Hamilton,Lab Director <br /> i <br />