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I I 10 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax : 925-798-1622 <br /> Fes" hhM://www.rnccu=bell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Geweke <br /> Date Sampled: 03/17/99 <br /> 4005 North Wilson Way Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 03/21-03/24/99 <br />' [Client P.O: Date Analyzed: 03/21-03/24/99 <br /> Volatile Organics By GC/MS <br />' EPA method 8260 <br /> Lab ID 05373 <br /> Client ID EW-1 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<3 Ethylbenzene NO <br />' Benzene NO Hexachlorobutadiene NO <br /> Bromobenzene NO lodomethane NO <br /> Bromochloromethane ND Isopropylbenzene NO <br /> Bromodichloromethane NO p-Isopropyl toluene NO <br />' Bromoform NO Methyl butyl ketone NO <br /> Bromomcthane NO Methylene Chloride"' ND <br /> n-Butyl benzene NO Methyl ethyl ketone NO <br /> sec-Butyl benzene ND Methyl isobutyl ketones NO <br />' tert-Butyl benzene NO Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene NO <br /> Carbon Tetrachloride NO n-Propyl benzene NO <br /> Chlorobenzene NO Styrene ND <br /> Chloroethane NO 1.1,1,2-Tetrachloroethane NO <br /> 2-Chloroethyl Vinyl Ether` NO 1,1,2,2-Tetrachloroethane NO <br /> Chloroform NO Tetrachloroethane NO <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene NO 1,2,3-Trichlorobenzene NO <br /> 4-Chlorotoiuene NO 1,2,4-Trichlorobenzcne NO <br /> Dibromocbloromethane NO 1,1,1-Trichloroethane NO <br /> I 1,2-Dibromo-3-chloropropane NO 1,1,2-Trichloroethane NO <br /> Dibromomethane NO Trichloroethene NO <br /> 1,2-Dichlorobenzene NO Trichlorofluoromethane NO <br /> 1,3-Dichlorobenzene NO 1,2,3-Trichloropropane ND <br />' 1,4-Dichlorobenzene NO 1,2,4-Trimethylbenzene NO <br /> Dichlorodifluoromethane NO 1,3,5-Trimethylbenzene NO <br /> I,I-Dichloroethane NO Vinyl Acetate" NO <br /> 1,2-Dichloroethane 8.9 Vinyl Chloride`" NO <br /> I,1-Dichloroethene NO Xylenes,total NO <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane NO <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane NO Comments: <br /> 1,1-Dichloropropene NO Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene NO Dibromofluoromethane 92 <br />' trans-1,3-Dichloropropene ND Toluene-d8 111 <br /> Ethylene dibromide NO 4-Bromofluorobenzene 121 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/NAlpe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe NO means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 // Edward Hamilton,Lab Director <br /> I <br />